IRON Laboratories

Marihuana Potency Analysis by
Gas Chromatography
Test Certificate #: 420-001
Client Name, Sample Details

David Esser
Allen Park, MI 48101
Sample: Blue Dream
Type: Flower
Method: FE03 HP5890-1
Test Conditions

Sample ID#: 420

Harvest/Process Date: 07/26/2011
Date Received: 07/26/2011
Test Date: 07/26/2011
Valid Through: 07/26/2012
Report Issued: 07/26/2011
Sample #420
Test
Compounds		 CBDV THCV CBC CBD Δ8 THC Δ9 THC CBG CBN TOTAL
Amount N/D N/D N/D 0.4 N/D 21.1 N/D 0.6 22.0%
Min. Value 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% -
Uncertainty† ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD -

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; N/D = Not Detected

*** Designated tests that use the method FE-45.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Makenzie Hyman Iron laboratories Makenzie Hyman

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 420-001
Client Name, Sample Details

David Esser
Allen Park, MI 48101
Sample: Blue Dream
Type: Flower
Method: FE04-OR4 HPLC1100-OR1
***Moisture: 9.36%
Test Conditions

Prepsheet ID#: P180710a
Scale: XS205-OR1
Temp: 21.4 °C
Baro Pressure: 1007 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 420

Harvest/Process Date: 07/26/2011
Date Received: 07/26/2011
Test Date: 07/10/2018
Sample #420
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV Total THC Total CBD
Amount N/D 3.51% 0.48% 0.09% 0.16% 0.08% 3.10% 14.41% N/D 15.74% 3.56%
LOQ 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05%
Uncertainty 2.07% RPD 1.35% RPD 3.00% RPD 0.81% RPD 2.96% RPD 2.21% RPD ±5% RPD 3.32% RPD 1.62% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 420-001
Client Name, Sample Details

David Esser
Allen Park, MI 48101
Sample: Blue Dream
Type: Flower
Method: FE04-OR4 HPLC1100-OR1
***Moisture: 9.36%
Test Conditions

Prepsheet ID#: P180710a
Scale: XS205-OR1
Temp: 21.4 °C
Baro Pressure: 1007 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 420

Harvest/Process Date: 07/26/2011
Date Received: 07/26/2011
Test Date: 07/10/2018
Sample #420
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.97 4.88 98.19 4.78 96.18 2.07%
Cannabidiolic Acid (CBDA) N.D. 5.07 5.21 102.76 5.14 101.38 1.35%
Cannabigerol (CBG) N.D. 4.81 4.8 99.79 4.66 96.88 2.96%
Cannabidiol (CBD) N.D. 5.13 5.08 99.03 4.93 96.10 3.00%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 4.98 4.97 99.80 4.89 98.19 1.62%
Cannabinol (CBN) N.D. 5.14 5.04 98.05 4.93 95.91 2.21%
Δ9-Tetrahydrocannabinol (THC) N.D. 4.96 4.69 94.56 4.59 92.54 2.16%
Cannabichromene (CBC) N.D. 5.28 4.94 93.56 4.9 92.80 0.81%
Tetrahydrocannabinolic acid (THCA) N.D. 5.21 5.2 99.81 5.03 96.55 3.32%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 420-001
Client Name, Sample Details

David Esser
Allen Park, MI 48101
Sample: Blue Dream
Type: Flower
Method: FE04-OR4 HPLC1100-OR1
***Moisture: 9.38%
Test Conditions

Prepsheet ID#: P180710a
Scale: XS205-OR1
Temp: 21.4 °C
Baro Pressure: 1007 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 420

Harvest/Process Date: 07/26/2011
Date Received: 07/26/2011
Test Date: 07/10/2018
Sample #420
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV Total THC Total CBD
Amount N/D 1.91% 0.25% 0.10% 0.16% 0.09% 3.67% 16.87% N/D 18.46% 1.92%
LOQ 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05%
Uncertainty 2.07% RPD 1.35% RPD 3.00% RPD 0.81% RPD 2.96% RPD 2.21% RPD ±5% RPD 3.32% RPD 1.62% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 420-001
Client Name, Sample Details

David Esser
Allen Park, MI 48101
Sample: Blue Dream
Type: Flower
Method: FE04-OR4 HPLC1100-OR1
***Moisture: 9.38%
Test Conditions

Prepsheet ID#: P180710a
Scale: XS205-OR1
Temp: 21.4 °C
Baro Pressure: 1007 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 420

Harvest/Process Date: 07/26/2011
Date Received: 07/26/2011
Test Date: 07/10/2018
Sample #420
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.97 4.88 98.19 4.78 96.18 2.07%
Cannabidiolic Acid (CBDA) N.D. 5.07 5.21 102.76 5.14 101.38 1.35%
Cannabigerol (CBG) N.D. 4.81 4.8 99.79 4.66 96.88 2.96%
Cannabidiol (CBD) N.D. 5.13 5.08 99.03 4.93 96.10 3.00%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 4.98 4.97 99.80 4.89 98.19 1.62%
Cannabinol (CBN) N.D. 5.14 5.04 98.05 4.93 95.91 2.21%
Δ9-Tetrahydrocannabinol (THC) N.D. 4.96 4.69 94.56 4.59 92.54 2.16%
Cannabichromene (CBC) N.D. 5.28 4.94 93.56 4.9 92.80 0.81%
Tetrahydrocannabinolic acid (THCA) N.D. 5.21 5.2 99.81 5.03 96.55 3.32%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 4
IRON Laboratories

Bio Analysis by
Gas Chromatography
Test Certificate #: 420-001
Client Name, Sample Details

David Esser
Allen Park, MI 48101
Sample: Blue Dream
Type: Flower
Method: FE03 HP5890-1
Test Conditions

Sample ID#: 420

Harvest/Process Date: 07/26/2011
Date Received: 07/26/2011
Test Date: 07/26/2011
Valid Through: 07/26/2012
Report Issued: 07/26/2011
Sample #420
Impurities: Not Detected
Molds: No Types: N/A
Pests: No Types: N/A
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture -

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 4