IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 152017-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 1g AIO-Sour Diesel
License: AU-P-000253
Type: AU Vape Cart
Method: FE04U12 HPLC-UV
Metrc Test Pkg#: 1A405030002A686000229873
Metrc Source Pkg#: 1A405030002A686000217253

Test Conditions

Prepsheet ID#: MIP241213b
Scale: XS205-MI1
Temp: 21.2 °C
Baro Pressure: 978.3 hPa
Analyst: MEH
Technician: ARH

Sample ID#: 152017

Harvest/Process Date: 12/16/2024
Serving Size (g): 1
Date Received: 12/16/2024
Test Date: 12/13/2024
Valid Through: 12/14/2025
Report Issued: 12/18/2024

Sample #152017
Sample #152017 Sample #152017
Test
Compounds
Δ9-THC THCA Δ8-THC CBD CBDA CBG CBGA CBN CBC CBL THCV CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 85.3 N/D N/D 0.4 N/D 2.5 N/D 0.9 0.4 N/D 0.5 N/D 90.1 85.3 0.4 90.1
Amount (mg/g) 853.2 N/D N/D 4.4 N/D 25.3 N/D 9.0 3.8 N/D 5.1 N/D 900.8 853.2 4.4 900.8
Amount per Serving (mg) 853.2 N/D N/D 4.4 N/D 25.3 N/D 9 3.8 N/D 5.1 N/D 900.8  
LOQ (mg/g) 2.93 2.93 2.93 2.93 2.93 2.93 2.93 2.93 2.93 2.93 2.93 2.93   %Decarb. THC CBD
±%RPD 0.40% 2.55% 0.92% 0.31% 0.07% 0.04% 0.89% 0.30% 0.69% 0.07% 1.13% 0.19% 100% 100%

Sample tested for potency and vitamin E acetate. Sample does not contain vitamin E acetate over 100 ug/g (PASS). C6 Pass; C8 Pass; C10 Pass; C12 Pass; Target MCTs (C6, C8, C10, and C12) have individual action limits of 100 ppm (Pass = Less than 100 ppm; Fail = Greater than or Equal to 100 ppm). MCTs are analyzed utilizing FE-70 (HPLC-UV) with a relative expanded (k=2) uncertainty of 20%.

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected. *Designates values that are not currently included in the accredited scope of Iron Laboratories. *** Designates tests that use the SOP FE-45 (water activity meter) method. FE-45 is performed using AOAC 966.02 and 32.004-32.009.

FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products.

Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%. Sample fails vitamin E acetate if VEA>100 ug/g.

Total THC and CBD is the calculated sum of Δ9-THC and Δ8-THC or CBD plus the amount of THC or CBD derived from THCA or CBDA, respectively.

These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, Total CBG, CBC, THCV, CBDV, and CBL. Total CBG is calculated as CBG plus CBGA*0.878 (the molar correction factor for CBGA to CBG conversion). %Decarb. THC and CBD refer to the percentage of Δ9-THC or CBD relative to THCA or CBDA, respectively.

Potency Action Limits
Product Type Action Limit
Concentrates & Vapes Delta-8 concentration cannot exceed 10%
Infused Products

Delta-8 cannot exceed 10% of the maximum THC limits;

Homogeneity must be ≤15% RSD; Variance must be ≤10%

Maximum THC (Sum of Delta-8 and Delta-9) Concentrations for Infused Products (in mg)

 Category

Medical

(Per Dose)

Medical

(Per Container)

Adult-Use

(Per Dose)

Adult-Use

(Per Container)

Infused edibles (gummies, baked goods, drink enhancers, syrup) 50 200 10 200
Medicinal products (capsules, tinctures, oil-based drops) 100 2000 10 200
Medicinal Products not consumed orally (suppositories, tampons, transdermal patches) 100 2000 100 2000
Beverages 10 100 10 100

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 6

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 152017-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 1g AIO-Sour Diesel
License: AU-P-000253
Type: AU Vape Cart
Method: FE04U12 HPLC-UV
Metrc Test Pkg#: 1A405030002A686000229873
Metrc Source Pkg#: 1A405030002A686000217253

Test Conditions

Prepsheet ID#: MIP241213b
Scale: XS205-MI1
Temp: 21.2 °C
Baro Pressure: 978.3 hPa
Analyst: MEH
Technician: ARH

Sample ID#: 152017

Harvest/Process Date: 12/16/2024
Serving Size (g): 1
Date Received: 12/16/2024
Test Date: 12/13/2024
Valid Through: 12/14/2025
Report Issued: 12/18/2024

Sample #152017
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Δ9-THC 0 5.15448 5.16821 100.27 5.14779 99.87 0.40%
THCA 0 5.22718 5.00582 95.77 5.13496 98.24 2.55%
Δ8-THC 0 5.13529 5.01598 97.68 5.0622 98.58 0.92%
CBD 0 6.14608 5.05724 82.28 5.07271 82.54 0.31% LR
CBDA 0 5.02567 5.03867 100.26 5.04245 100.33 0.07%
CBG 0 5.2129 5.03152 96.52 5.03353 96.56 0.04%
CBGA 0 5.00582 5.03331 100.55 4.98875 99.66 0.89%
CBN 0 5.09493 5.0686 99.48 5.08367 99.78 0.30%
CBC 0 4.98278 4.9818 99.98 4.94747 99.29 0.69%
CBCA N/A 0 0 0.00 0 0.00 0% N/A
CBL 0 4.99775 4.93663 98.78 4.93995 98.84 0.07%
THCV 0 5.05611 5.03206 99.52 4.97531 98.40 1.13%
CBDV 0 4.97029 4.94466 99.48 4.9543 99.68 0.19%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 6

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 77802 Test Certificate #: 152017-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 1g AIO-Sour Diesel
License: AU-P-000253
Type: AU Vape Cart
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A405030002A686000229873
Metrc Source Pkg#: 1A405030002A686000217253

Test Conditions

Prepsheet ID#: MIPS241218b
Scale: XS205-MI1
Temp: 21.3 °C
Baro PE: 980.3 hPa
Analyst: OSB
Technician: OSB

Sample ID#: 152017

Harvest/Process Date: 12/16/2024
Serving Size (g): 1
Date Received: 12/16/2024
Test Date: 12/18/2024
Valid Through: 12/18/2025
Report Issued: 12/20/2024

Sample #152017
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.200 Pass/<LOD Abamectin**** 0.500 0.250 Pass/<LOD
Acephate 0.400 0.200 Pass/<LOD Acequinocyl 2.000 1.000 Pass/<LOD
Acetamiprid 0.200 0.100 Pass/<LOD Azoxystrobin 0.200 0.100 Pass/<LOD
Bifenazate 0.200 0.100 Pass/<LOD Bifenthrin 0.200 0.100 Pass/<LOD
Boscalid 0.400 0.200 Pass/<LOD Carbaryl 0.200 0.100 Pass/<LOD
Carbofuran 0.200 0.100 Pass/<LOD Chlorantraniliprole 0.200 0.100 Pass/<LOD
Chlorfenapyr 1.000 0.500 Pass/<LOD Chlorpyrifos 0.200 0.100 Pass/<LOD
Clofentezine 0.200 0.100 Pass/<LOD Cyfluthrin** 1.000 0.500 Pass/<LOD
Cypermethrin*** 1.000 0.500 Pass/<LOD Daminozide 1.000 0.500 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.500 Pass/<LOD Diazinon 0.200 0.100 Pass/<LOD
Dimethoate 0.200 0.100 Pass/<LOD Ethoprophos 0.200 0.100 Pass/<LOD
Etofenprox 0.400 0.200 Pass/<LOD Etoxazole 0.200 0.100 Pass/<LOD
Fenoxycarb 0.200 0.100 Pass/<LOD Fenpyroximate 0.400 0.200 Pass/<LOD
Fipronil 0.400 0.200 Pass/<LOD Flonicamid 1.000 0.500 Pass/<LOD
Fludioxonil 0.400 0.200 Pass/<LOD Hexythiazox 1.000 0.500 Pass/<LOD
Imazalil 0.200 0.100 Pass/<LOD Imidacloprid 0.400 0.200 Pass/<LOD
Kresoxim Methyl 0.400 0.200 Pass/<LOD Malathion 0.200 0.100 Pass/<LOD
Metalaxyl 0.200 0.100 Pass/<LOD Methiocarb 0.200 0.100 Pass/<LOD
Methomyl 0.400 0.200 Pass/<LOD Methyl Parathion 0.200 0.100 Pass/<LOD
MGK-264‡ 0.200 0.100 Pass/<LOD Myclobutanil 0.200 0.100 Pass/<LOD
Naled 0.500 0.250 Pass/<LOD Oxamyl 1.000 0.500 Pass/<LOD
Paclobutrazol 0.400 0.200 Pass/<LOD Permethrins† 0.200 0.100 Pass/<LOD
Phosmet 0.200 0.100 Pass/<LOD Piperonyl Butoxide 100.000 1.900 Not Tested
Prallethrin 0.200 0.100 Pass/<LOD Propiconazole 0.400 0.200 Pass/<LOD
Propoxur 0.200 0.100 Pass/<LOD Pyrethrins* 1.000 0.500 Pass/<LOD
Pyridaben 0.200 0.100 Pass/<LOD Spinosad***** 0.200 0.100 Pass/<LOD
Spiromesifen 0.200 0.100 Pass/<LOD Spirotetramat 0.200 0.100 Pass/<LOD
Spiroxamine‡ 0.400 0.200 Pass/<LOD Tebuconazole 0.400 0.200 Pass/<LOD
Thiacloprid 0.200 0.100 Pass/<LOD Thiamethoxam 0.200 0.100 Pass/<LOD
Trifloxystrobin 0.200 0.100 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 6

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Pesticide QC Report

Testing Accreditation #: 77802 Test Certificate #: 152017-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 1g AIO-Sour Diesel
License: AU-P-000253
Type: AU Vape Cart
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A405030002A686000229873
Metrc Source Pkg#: 1A405030002A686000217253

Test Conditions

Prepsheet ID#: MIPS241218b
Scale: XS205-MI1
Temp: 21.3 °C
Baro PE: 980.3 hPa
Analyst: OSB
Technician: OSB

Sample ID#: 152017

Harvest/Process Date: 12/16/2024
Serving Size (g): 1
Date Received: 12/16/2024
Test Date: 12/18/2024
Valid Through: 12/18/2025
Report Issued: 12/20/2024

Sample #152017
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.55 1.93 155.00 193.00 21.84 HR
Acequinocyl N.D. 1 1.2 0.895 120.00 89.50 29.12
Acetamiprid N.D. 1 1.35 1.27 135.00 127.00 6.11 HR
Aldicarb N.D. 1 1.29 1.26 129.00 126.00 2.35 HR
Avermectin B1a N.D. 1 1.23 0.932 123.00 93.20 27.57 HR
Azoxystrobin N.D. 1 0.946 0.854 94.60 85.40 10.22
Bifenazate N.D. 1 0.68 1.1 68.00 110.00 47.19 Q
Bifenthrin N.D. 1 1.14 0.964 114.00 96.40 16.73
Boscalid N.D. 1 1.3 1.75 130.00 175.00 29.51 HR
Carbaryl N.D. 1 1.37 1.38 137.00 138.00 0.73 HR
Carbofuran N.D. 1 1.31 1.23 131.00 123.00 6.30 HR
Chlorantraniliprole N.D. 1 0.532 0.896 53.20 89.60 50.98 LRQ
Chlorfenapyr N.D. 1 1.01 0.614 101.00 61.40 48.77 Q
Chlorpyriphos N.D. 1 1.26 1.4 126.00 140.00 10.53 HR
Clofentezine N.D. 1 0.675 1 67.50 100.00 38.81 Q
Cyfluthrin N.D. 1 0.69 0.835 69.00 83.50 19.02
Cypermethrin N.D. 1 0.789 0.788 78.90 78.80 0.13
Daminoside N.D. 1 0.0489 0.0572 4.89 5.72 15.65 LR
Diazanon N.D. 1 1.01 1.72 101.00 172.00 52.01 HRQ
Dichlorvos N.D. 1 1.48 1.27 148.00 127.00 15.27 HR
Dimethoate N.D. 1 1.33 1.2 133.00 120.00 10.28 HR
Ethoprophos N.D. 1 1.58 1.45 158.00 145.00 8.58 HR
Etofenprox N.D. 1 1.41 0.807 141.00 80.70 54.40 HRQ
Etoxazole N.D. 1 1.2 1.15 120.00 115.00 4.26
Fenoxycarb N.D. 1 0.8 0.927 80.00 92.70 14.71
Fenpyroximate N.D. 1 0.895 0.824 89.50 82.40 8.26
Fipronil N.D. 1 0.919 0.89 91.90 89.00 3.21
Flonicamid N.D. 1 1.4 1.23 140.00 123.00 12.93 HR
Fludioxonil N.D. 1 0.859 0.987 85.90 98.70 13.87
Hexythiazox N.D. 1 1.33 1.26 133.00 126.00 5.41 HR
Imazalil N.D. 1 0.431 0.711 43.10 71.10 49.04 LRQ
Imidacloprid N.D. 1 0.87 0.973 87.00 97.30 11.18
Kresoxim-methyl N.D. 1 1.06 1.97 106.00 197.00 60.07 HRQ
Malathion N.D. 1 1.13 1.59 113.00 159.00 33.82 HRQ
Metalaxyl N.D. 1 0.585 0.826 58.50 82.60 34.16 LRQ
Methiocarb N.D. 1 1.3 1.13 130.00 113.00 13.99 HR
Methomyl N.D. 1 1.11 1.67 111.00 167.00 40.29 HRQ
MGK-264 N.D. 1 0.529 0.656 52.90 65.60 21.43 LR
Myclobutanil N.D. 1 0.475 0.722 47.50 72.20 41.27 LRQ
Naled (dibrom) N.D. 1 0.681 0.683 68.10 68.30 0.29
Oxamyl N.D. 1 1.47 1.22 147.00 122.00 18.59 HR
Paclobutrazol N.D. 1 0.626 1.04 62.60 104.00 49.70 Q
Parathion-methyl N.D. 1 0.955 1.41 95.50 141.00 38.48 HRQ
Permethrins N.D. 1 1.071 0.667 107.10 66.70 46.49 Q
Phosmet N.D. 1 1.11 1.48 111.00 148.00 28.57 HR
Piperonyl butoxide N/A N/A N/A N/A nan nan N/A
Prallethrin N.D. 1 0.84 1.23 84.00 123.00 37.68 HRQ
Propiconazole N.D. 1 1.4 1.55 140.00 155.00 10.17 HR
Propoxur N.D. 1 1.29 1.21 129.00 121.00 6.40 HR
Pyrethrin N.D. 1 1.46 2.02 146.00 202.00 32.18 HRQ
Pyridaben N.D. 1 1.49 1.1 149.00 110.00 30.12 HRQ
SpinosynA N.D. 0.82 0.443 0.637 54.02 77.68 35.93 LRQ
SpinosynD N.D. 0.18 0.146 0.233 81.11 129.44 45.91 HRQ
Spiromesifen N.D. 1 0.945 0.848 94.50 84.80 10.82
Spirotetramat N.D. 1 1.3 1.22 130.00 122.00 6.35 HR
Spiroxamine N.D. 1 0.624 0.874 62.40 87.40 33.38 Q
Tebuconazole N.D. 1 0.835 1.43 83.50 143.00 52.54 HRQ
Thiacloprid N.D. 1 0.862 0.951 86.20 95.10 9.82
Thiamethoxam N.D. 1 0.639 1.1 63.90 110.00 53.02 Q
Trifloxystrobin N.D. 1 1.22 0.983 122.00 98.30 21.52 HR

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 6

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Residual Solvents Analysis by
Mass Spectrometer

Testing Accreditation #: 77802 Test Certificate #: 152017-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 1g AIO-Sour Diesel
License: AU-P-000253
Type: AU Vape Cart
Method: SOP FE-44-MI
Metrc Test Pkg#: 1A405030002A686000229873
Metrc Source Pkg#: 1A405030002A686000217253

Test Conditions

Prepsheet ID#: MIHS241218a
Scale: XS205-MI1
Temp: 22.9 °C
Baro PE: 976.9 hPa
Analyst: OSB
Technician: OSB

Sample ID#: 152017

Harvest/Process Date: 12/16/2024
Serving Size (g): 1
Date Received: 12/16/2024
Test Date: 12/18/2024
Valid Through: 12/18/2025
Report Issued: 12/19/2024

Sample #152017
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 5,000 250 Not Tested
1,4-dioxane 5,000 25 Not Tested 1-Butanol 5,000 250 Not Tested
1-Pentanol 5,000 250 Not Tested 1-Propanol 5,000 250 Not Tested
2,2-Dimethylpropane (Neopentane) 750 25 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 50 25 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 50 25 Pass/<LOD 2-Butanol 5,000 25 Not Tested
2-Butanone (MEK) 5,000 250 Not Tested 2-Ethoxyethanol 5,000 25 Not Tested
2-Methylbutane (Isopentane) 750 25 Pass/<LOD 2-Methylpentane (Hexanes) 50 25 Pass/<LOD
2-Methylpropane (Isobutane) 800 25 Pass/<LOD 2-propanol (Isopropyl Alcohol) 500 25 Pass/<LOD
2-Propanone (Acetone) 750 25 Pass/<LOD 3-Methylpentane (Hexanes) 50 25 Pass/<LOD
Acetonitrile 60 30 Pass/<LOD Benzene 1 1 Pass/<LOD
Butane 800 25 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 5,000 25 Not Tested Cyclohexane 50 25 Not Tested
Dichloromethane 125 25 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 250 Not Tested
Ethanol 1,000 50 Pass/<LOD Ethyl acetate 400 25 Pass/<LOD
Ethyl ether 500 25 Pass/<LOD Ethylene glycol 5,000 25 Not Tested
Ethylene oxide 5 3 Pass/<LOD Heptane 500 25 Pass/<LOD
Hexane 50 25 Pass/<LOD Isopropyl acetate 5,000 25 Not Tested
Methanol 250 125 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 5,000 250 Not Tested N,N-Dimethylformamide (DMF) 5,000 250 Not Tested
Pentane 750 25 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 2,100 25 Pass/<LOD Pyridine 5,000 250 Not Tested
Sulfolane 5,000 25 Not Tested Tetrahydrofuran (THF) 5,000 25 Not Tested
Toluene 150 25 Pass/<LOD Trichloroethylene 25 10 Pass/<LOD
Xylenes* 150 25 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 6

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Residual Solvents QC Report

Testing Accreditation #: 77802 Test Certificate #: 152017-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 1g AIO-Sour Diesel
License: AU-P-000253
Type: AU Vape Cart
Method: SOP FE-44-MI
Metrc Test Pkg#: 1A405030002A686000229873
Metrc Source Pkg#: 1A405030002A686000217253

Test Conditions

Prepsheet ID#: MIHS241218a
Scale: XS205-MI1
Temp: 22.9 °C
Baro PE: 976.9 hPa
Analyst: OSB
Technician: OSB

Sample ID#: 152017

Harvest/Process Date: 12/16/2024
Serving Size (g): 1
Date Received: 12/16/2024
Test Date: 12/18/2024
Valid Through: 12/18/2025
Report Issued: 12/19/2024

Sample #152017
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 250 273 304 109.20 121.60 10.75
n-Propane N.D. 250 207 182 82.80 72.80 12.85
Isobutane N.D. 250 196 200 78.40 80.00 2.02
Methanol N.D. 250 176 188 70.40 75.20 6.59
n-Butane N.D. 250 199 204 79.60 81.60 2.48
2,2-Dimethylpropane N.D. 250 201 233 80.40 93.20 14.75
Ethanol N.D. 250 196 235 78.40 94.00 18.10
Isopentane N.D. 250 201 232 80.40 92.80 14.32
Acetonitrile N.D. 250 189 220 75.60 88.00 15.16
Diethyl ether N.D. 250 219 244 87.60 97.60 10.80
2-propanone N.D. 250 196 241 78.40 96.40 20.59 Q
2-propanol N.D. 250 221 255 88.40 102.00 14.29
n-Pentane N.D. 250 201 238 80.40 95.20 16.86
2,2-Dimethylbutane N.D. 250 209 246 83.60 98.40 16.26
2,3-Dimethylbutane N.D. 250 231 259 92.40 103.60 11.43
Methylene chloride N.D. 250 214 246 85.60 98.40 13.91
2-Methylpentane N.D. 250 216 248 86.40 99.20 13.79
3-Methylpentane N.D. 250 212 247 84.80 98.80 15.25
2-Butanol N.D. 0 0 0 0.00 0.00 0.00
n-Hexane N.D. 250 214 251 85.60 100.40 15.91
Ethyl acetate N.D. 250 216 253 86.40 101.20 15.78
Tetrahydrofuran N.D. 0 0 0 0.00 0.00 0.00
Trichloroethylene N.D. 250 255 279 102.00 111.60 8.99
Isopropyl acetate N.D. 0 0 0 0.00 0.00 0.00
Benzene N.D. 250 230 263 92.00 105.20 13.39
Chloroform N.D. 250 257 291 102.80 116.40 12.41
Cyclohexane N.D. 0 0 0 0.00 0.00 0.00
Ethylene glycol N.D. 0 0 0 0.00 0.00 0.00
Heptane N.D. 250 224 252 89.60 100.80 11.76
2-Ethoxyethanol N.D. 0 0 0 0.00 0.00 0.00
1,4-Dioxane N.D. 0 0 0 0.00 0.00 0.00
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 243 288 97.20 115.20 16.95
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 0 0 0 0.00 0.00 0.00
m-Xylene/p-Xylene N.D. 500 530 609 106.00 121.80 13.87
o-Xylene N.D. 250 270 310 108.00 124.00 13.79
Cumene N.D. 0 0 0 0.00 0.00 0.00
Ethylene oxide N.D. 250 192 226 76.80 90.40 16.27

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 6

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Heavy Metals Analysis

Testing Accreditation #: 77802 Test Certificate #: 152017-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 1g AIO-Sour Diesel
License: AU-P-000253
Type: AU Vape Cart
Method: FE60 ICPMS-MI
Metrc Test Pkg#: 1A405030002A686000229873
Metrc Source Pkg#: 1A405030002A686000217253

Test Conditions

Prepsheet ID#: HMMIICP241216cMK
Temp: 23.0 °C
Baro PE: 974.4 hPa
Analyst: MK
Technician: MK

Sample ID#: 152017

Harvest/Process Date: 12/16/2024
Serving Size (g): 1
Date Received: 12/16/2024
Test Date: 12/16/2024
Valid Through: 12/16/2025
Report Issued: 12/17/2024

Sample #152017
Sample #152017 Sample #152017
Test Compound MRL (PPM) LOD (PPM) Status (PPM)
Arsenic 0.2 0.1 Pass/<LOD
Copper 3 1.5 Pass/<LOD
Cadmium 0.2 0.1 Pass/<LOD
Chromium 0.6 0.3 Pass/<LOD
Lead 0.5 0.25 Pass/<LOD
Mercury 0.1 0.05 Pass/<LOD
Nickel 0.5 0.25 Pass/<LOD

MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 6 of 6

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 152017-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 1g AIO-Sour Diesel
License: AU-P-000253
Type: AU Vape Cart
Method: FE60 ICPMS-MI
Metrc Test Pkg#: 1A405030002A686000229873
Metrc Source Pkg#: 1A405030002A686000217253

Test Conditions

Prepsheet ID#: HMMIICP241216cMK
Temp: 23.0 °C
Baro PE: 974.4 hPa
Analyst: MK
Technician: MK

Sample ID#: 152017

Harvest/Process Date: 12/16/2024
Serving Size (g): 1
Date Received: 12/16/2024
Test Date: 12/16/2024
Valid Through: 12/16/2025
Report Issued: 12/17/2024

Sample #152017
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD QC Flag
Arsenic N/D 0.160 0.158 98.75 0.165 103.13
Cadmium N/D 0.160 0.150 93.75 0.161 100.63
Chromium N/D 0.480 0.288 60.00 0.292 60.83
Copper N/D 2.400 2.421 100.88 2.470 102.92
Lead N/D 0.400 0.406 101.50 0.415 103.75
Mercury N/D 0.080 0.073 91.25 0.085 106.25
Nickel N/D 0.400 0.391 97.75 0.408 102.00

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 7 of 6