IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 145844-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 2.5g PR Multipack-Pink Acai
License: AU-P-000253
Type: AU Infused Pre-Roll W/Solvents
Method: FE04 HPLC-UV
Metrc Test Pkg#: 1A405030002A686000155310
Metrc Source Pkg#: 1A405030002A686000155209
***Water Activity: 0.39

Test Conditions

Prepsheet ID#: MIP240304a
Scale: XS205-MI2
Temp: 23.5 °C
Baro Pressure: 979.9 hPa
Analyst: MEH
Technician: ARH

Sample ID#: 145844

Harvest/Process Date: 03/04/2024
Serving Size (g): 1
Date Received: 03/04/2024
Test Date: 03/04/2024
Valid Through: 03/05/2025
Report Issued: 03/05/2024

Sample #145844
Sample #145844 Sample #145844
Test
Compounds
Δ9-THC THCA Δ8-THC CBD CBDA CBG CBGA CBN CBC CBL THCV CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 30.6 16.0 N/D N/D N/D 1.1 0.5 0.2 0.8 N/D 0.4 N/D 49.4 44.6 0.0 47.4
Amount (mg/g) 306.0 159.7 N/D N/D N/D 10.6 4.62 1.9 7.6 N/D 3.9 N/D 494.32 446.1 0.0 474.1
Amount per Serving (mg) 306 159.7 N/D N/D N/D 10.6 4.62 1.9 7.6 N/D 3.9 N/D 494.3  
LOQ (mg/g) 1.83 1.83 1.83 1.83 1.83 1.83 1.83 1.83 1.83 1.83 1.83 1.83   %Decarb. THC CBD
±%RPD 2.61% 1.19% 2.28% 0.22% 0.54% 0.39% 0.63% 0.87% 0.55% 1.51% 0.77% 0.16% 66 N/A

Sample passes for water activity (sample fails if Aw>0.65). Water activity is measured utilizing SOP FE-45 (water activity meter).

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected. *Designates values that are not currently included in the accredited scope of Iron Laboratories. *** Designates tests that use the SOP FE-45 (water activity meter) method. FE-45 is performed using AOAC 966.02 and 32.004-32.009.

FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products.

Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%. Sample fails vitamin E acetate if VEA>100 ug/g.

Total THC and CBD is the calculated sum of Δ9-THC and Δ8-THC or CBD plus the amount of THC or CBD derived from THCA or CBDA, respectively.

These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, Total CBG, CBC, THCV, CBDV, and CBL. Total CBG is calculated as CBG plus CBGA*0.878 (the molar correction factor for CBGA to CBG conversion). %Decarb. THC and CBD refer to the percentage of Δ9-THC or CBD relative to THCA or CBDA, respectively.

Potency Action Limits
Product Type Action Limit
Concentrates & Vapes Delta-8 concentration cannot exceed 10%
Infused Products

Delta-8 cannot exceed 10% of the maximum THC limits;

Homogeneity must be ≤15% RSD; Variance must be ≤10%

Maximum THC (Sum of Delta-8 and Delta-9) Concentrations for Infused Products (in mg)

 Category

Medical

(Per Dose)

Medical

(Per Container)

Adult-Use

(Per Dose)

Adult-Use

(Per Container)

Infused edibles (gummies, baked goods, drink enhancers, syrup) 50 200 10 200
Medicinal products (capsules, tinctures, oil-based drops) 100 2000 10 200
Medicinal Products not consumed orally (suppositories, tampons, transdermal patches) 100 2000 100 2000
Beverages 10 100 10 100

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information. AU License #: AU-SC-000107; MED License #: SC-000003.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 8

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 145844-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 2.5g PR Multipack-Pink Acai
License: AU-P-000253
Type: AU Infused Pre-Roll W/Solvents
Method: FE04 HPLC-UV
Metrc Test Pkg#: 1A405030002A686000155310
Metrc Source Pkg#: 1A405030002A686000155209
***Water Activity: 0.39

Test Conditions

Prepsheet ID#: MIP240304a
Scale: XS205-MI2
Temp: 23.5 °C
Baro Pressure: 979.9 hPa
Analyst: MEH
Technician: ARH

Sample ID#: 145844

Harvest/Process Date: 03/04/2024
Serving Size (g): 1
Date Received: 03/04/2024
Test Date: 03/04/2024
Valid Through: 03/05/2025
Report Issued: 03/05/2024

Sample #145844
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Δ9-THC 0 4.87885 4.92679 100.98 4.79965 98.38 2.61%
THCA 0 4.99909 4.91126 98.24 4.85313 97.08 1.19%
Δ8-THC 0 5.34651 5.23113 97.84 5.11341 95.64 2.28%
CBD 0 5.09016 5.14713 101.12 5.15861 101.34 0.22%
CBDA 0 5.28756 5.29644 100.17 5.26785 99.63 0.54%
CBG 0 5.30762 5.27305 99.35 5.25237 98.96 0.39%
CBGA 0 5.14481 5.14893 100.08 5.11637 99.45 0.63%
CBN 0 5.11622 5.12485 100.17 5.16943 101.04 0.87%
CBC 0 5.1484 5.17913 100.60 5.20792 101.16 0.55%
CBCA N/A 0 0 0.00 0 0.00 0% N/A
CBL 0 5.25224 5.2664 100.27 5.18746 98.77 1.51%
THCV 0 5.59339 5.24772 93.82 5.20736 93.10 0.77%
CBDV 0 5.34951 5.25027 98.14 5.25867 98.30 0.16%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information. AU License #: AU-SC-000107; MED License #: SC-000003.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 8

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 77802 Test Certificate #: 145844-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 2.5g PR Multipack-Pink Acai
License: AU-P-000253
Type: AU Infused Pre-Roll W/Solvents
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A405030002A686000155310
Metrc Source Pkg#: 1A405030002A686000155209

Test Conditions

Prepsheet ID#: MIPS240304a
Scale: XS205-MI1
Temp: 22.6 °C
Baro PE: 989.2 hPa
Analyst: OSB
Technician: OSB

Sample ID#: 145844

Harvest/Process Date: 03/04/2024
Serving Size (g): 1
Date Received: 03/04/2024
Test Date: 03/04/2024
Valid Through: 03/04/2025
Report Issued: 03/05/2024

Sample #145844
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.200 Pass/<LOD Abamectin**** 0.500 0.250 Pass/<LOD
Acephate 0.400 0.200 Pass/<LOD Acequinocyl 2.000 1.000 Pass/<LOD
Acetamiprid 0.200 0.100 Pass/<LOD Azoxystrobin 0.200 0.100 Pass/<LOD
Bifenazate 0.200 0.100 Pass/<LOD Bifenthrin 0.200 0.100 Pass/<LOD
Boscalid 0.400 0.200 Pass/<LOD Carbaryl 0.200 0.100 Pass/<LOD
Carbofuran 0.200 0.100 Pass/<LOD Chlorantraniliprole 0.200 0.100 Pass/<LOD
Chlorfenapyr 1.000 0.500 Pass/<LOD Chlorpyrifos 0.200 0.100 Pass/<LOD
Clofentezine 0.200 0.100 Pass/<LOD Cyfluthrin** 1.000 0.500 Pass/<LOD
Cypermethrin*** 1.000 0.500 Pass/<LOD Daminozide 1.000 0.500 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.500 Pass/<LOD Diazinon 0.200 0.100 Pass/<LOD
Dimethoate 0.200 0.100 Pass/<LOD Ethoprophos 0.200 0.100 Pass/<LOD
Etofenprox 0.400 0.200 Pass/<LOD Etoxazole 0.200 0.100 Pass/<LOD
Fenoxycarb 0.200 0.100 Pass/<LOD Fenpyroximate 0.400 0.200 Pass/<LOD
Fipronil 0.400 0.200 Pass/<LOD Flonicamid 1.000 0.500 Pass/<LOD
Fludioxonil 0.400 0.200 Pass/<LOD Hexythiazox 1.000 0.500 Pass/<LOD
Imazalil 0.200 0.100 Pass/<LOD Imidacloprid 0.400 0.200 Pass/<LOD
Kresoxim Methyl 0.400 0.200 Pass/<LOD Malathion 0.200 0.100 Pass/<LOD
Metalaxyl 0.200 0.100 Pass/<LOD Methiocarb 0.200 0.100 Pass/<LOD
Methomyl 0.400 0.200 Pass/<LOD Methyl Parathion 0.200 0.100 Pass/<LOD
MGK-264‡ 0.200 0.100 Pass/<LOD Myclobutanil 0.200 0.100 Pass/<LOD
Naled 0.500 0.250 Pass/<LOD Oxamyl 1.000 0.500 Pass/<LOD
Paclobutrazol 0.400 0.200 Pass/<LOD Permethrins† 0.200 0.100 Pass/<LOD
Phosmet 0.200 0.100 Pass/<LOD Piperonyl Butoxide 100.000 1.900 Not Tested
Prallethrin 0.200 0.100 Pass/<LOD Propiconazole 0.400 0.200 Pass/<LOD
Propoxur 0.200 0.100 Pass/<LOD Pyrethrins* 1.000 0.500 Pass/<LOD
Pyridaben 0.200 0.100 Pass/<LOD Spinosad***** 0.200 0.100 Pass/<LOD
Spiromesifen 0.200 0.100 Pass/<LOD Spirotetramat 0.200 0.100 Pass/<LOD
Spiroxamine‡ 0.400 0.200 Pass/<LOD Tebuconazole 0.400 0.200 Pass/<LOD
Thiacloprid 0.200 0.100 Pass/<LOD Thiamethoxam 0.200 0.100 Pass/<LOD
Trifloxystrobin 0.200 0.100 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information. AU License #: AU-SC-000107; MED License #: SC-000003.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 8

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Pesticide QC Report

Testing Accreditation #: 77802 Test Certificate #: 145844-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 2.5g PR Multipack-Pink Acai
License: AU-P-000253
Type: AU Infused Pre-Roll W/Solvents
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A405030002A686000155310
Metrc Source Pkg#: 1A405030002A686000155209

Test Conditions

Prepsheet ID#: MIPS240304a
Scale: XS205-MI1
Temp: 22.6 °C
Baro PE: 989.2 hPa
Analyst: OSB
Technician: OSB

Sample ID#: 145844

Harvest/Process Date: 03/04/2024
Serving Size (g): 1
Date Received: 03/04/2024
Test Date: 03/04/2024
Valid Through: 03/04/2025
Report Issued: 03/05/2024

Sample #145844
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.22 1.32 122.00 132.00 7.87 HR
Acequinocyl N.D. 1 1.18 1.29 118.00 129.00 8.91 HR
Acetamiprid N.D. 1 1.33 1.48 133.00 148.00 10.68 HR
Aldicarb N.D. 1 1.09 1.2 109.00 120.00 9.61
Avermectin B1a N.D. 1 0.985 0.988 98.50 98.80 0.30
Azoxystrobin N.D. 1 1.4 1.54 140.00 154.00 9.52 HR
Bifenazate N.D. 1 1.27 1.3 127.00 130.00 2.33 HR
Bifenthrin N.D. 1 1.4 1.42 140.00 142.00 1.42 HR
Boscalid N.D. 1 1.44 1.55 144.00 155.00 7.36 HR
Carbaryl N.D. 1 1.3 1.35 130.00 135.00 3.77 HR
Carbofuran N.D. 1 1.51 1.55 151.00 155.00 2.61 HR
Chlorantraniliprole N.D. 1 1.43 1.59 143.00 159.00 10.60 HR
Chlorfenapyr N.D. 1 1.25 1.33 125.00 133.00 6.20 HR
Chlorpyriphos N.D. 1 1.3 1.44 130.00 144.00 10.22 HR
Clofentezine N.D. 1 1.29 1.41 129.00 141.00 8.89 HR
Cyfluthrin N.D. 1 1.31 1.43 131.00 143.00 8.76 HR
Cypermethrin N.D. 1 1.31 1.45 131.00 145.00 10.14 HR
Daminoside N.D. 1 1.2 0.995 120.00 99.50 18.68
Diazanon N.D. 1 3.79 4.15 379.00 415.00 9.07 HR
Dichlorvos N.D. 1 1.22 1.29 122.00 129.00 5.58 HR
Dimethoate N.D. 1 1.23 1.37 123.00 137.00 10.77 HR
Ethoprophos N.D. 1 1.21 1.44 121.00 144.00 17.36 HR
Etofenprox N.D. 1 1.42 1.56 142.00 156.00 9.40 HR
Etoxazole N.D. 1 1.49 1.61 149.00 161.00 7.74 HR
Fenoxycarb N.D. 1 1.52 1.67 152.00 167.00 9.40 HR
Fenpyroximate N.D. 1 1.49 1.68 149.00 168.00 11.99 HR
Fipronil N.D. 1 1.36 1.38 136.00 138.00 1.46 HR
Flonicamid N.D. 1 1.28 1.39 128.00 139.00 8.24 HR
Fludioxonil N.D. 1 1.16 1.21 116.00 121.00 4.22 HR
Hexythiazox N.D. 1 1.28 1.42 128.00 142.00 10.37 HR
Imazalil N.D. 1 1.32 1.52 132.00 152.00 14.08 HR
Imidacloprid N.D. 1 1.46 1.6 146.00 160.00 9.15 HR
Kresoxim-methyl N.D. 1 1.22 1.34 122.00 134.00 9.38 HR
Malathion N.D. 1 1.43 1.57 143.00 157.00 9.33 HR
Metalaxyl N.D. 1 1.48 1.56 148.00 156.00 5.26 HR
Methiocarb N.D. 1 1.4 1.48 140.00 148.00 5.56 HR
Methomyl N.D. 1 1.15 1.25 115.00 125.00 8.33 HR
MGK-264 N.D. 1 1.321 1.402 132.10 140.20 5.95 HR
Myclobutanil N.D. 1 1.51 1.79 151.00 179.00 16.97 HR
Naled (dibrom) N.D. 1 0.903 0.986 90.30 98.60 8.79
Oxamyl N.D. 1 1.34 1.5 134.00 150.00 11.27 HR
Paclobutrazol N.D. 1 1.42 1.6 142.00 160.00 11.92 HR
Parathion-methyl N.D. 1 0.869 0.978 86.90 97.80 11.80
Permethrins N.D. 1 1.327 1.453 132.70 145.30 9.06 HR
Phosmet N.D. 1 1.52 1.67 152.00 167.00 9.40 HR
Piperonyl butoxide N/A N/A N/A N/A nan nan N/A
Prallethrin N.D. 1 1.42 1.61 142.00 161.00 12.54 HR
Propiconazole N.D. 1 1.35 1.48 135.00 148.00 9.19 HR
Propoxur N.D. 1 1.26 1.39 126.00 139.00 9.81 HR
Pyrethrin N.D. 1 1.32 1.45 132.00 145.00 9.39 HR
Pyridaben N.D. 1 1.37 1.53 137.00 153.00 11.03 HR
SpinosynA N.D. 0.82 1.14 1.26 139.02 153.66 10.00 HR
SpinosynD N.D. 0.18 0.353 0.388 196.11 215.56 9.45 HR
Spiromesifen N.D. 1 1.05 1.17 105.00 117.00 10.81
Spirotetramat N.D. 1 1.34 1.48 134.00 148.00 9.93 HR
Spiroxamine N.D. 1 1.45 1.67 145.00 167.00 14.10 HR
Tebuconazole N.D. 1 1.48 1.68 148.00 168.00 12.66 HR
Thiacloprid N.D. 1 1.52 1.68 152.00 168.00 10.00 HR
Thiamethoxam N.D. 1 1.4 1.59 140.00 159.00 12.71 HR
Trifloxystrobin N.D. 1 1.29 1.44 129.00 144.00 10.99 HR

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information. AU License #: AU-SC-000107; MED License #: SC-000003.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 8

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Residual Solvents Analysis by
Mass Spectrometer

Testing Accreditation #: 77802 Test Certificate #: 145844-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 2.5g PR Multipack-Pink Acai
License: AU-P-000253
Type: AU Infused Pre-Roll W/Solvents
Method: SOP FE-44-MI (GCMS)
Metrc Test Pkg#: 1A405030002A686000155310
Metrc Source Pkg#: 1A405030002A686000155209

Test Conditions

Prepsheet ID#: MIHS240304a
Scale: XS205-MI1
Temp: 22.9 °C
Baro PE: 976.9 hPa
Analyst: OSB
Technician: OSB

Sample ID#: 145844

Harvest/Process Date: 03/04/2024
Serving Size (g): 1
Date Received: 03/04/2024
Test Date: 03/04/2024
Valid Through: 03/04/2025
Report Issued: 03/05/2024

Sample #145844
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 5,000 250 Not Tested
1,4-dioxane 5,000 25 Not Tested 1-Butanol 5,000 250 Not Tested
1-Pentanol 5,000 250 Not Tested 1-Propanol 5,000 250 Not Tested
2,2-Dimethylpropane (Neopentane) 750 25 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 50 25 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 50 25 Pass/<LOD 2-Butanol 5,000 25 Not Tested
2-Butanone (MEK) 5,000 250 Not Tested 2-Ethoxyethanol 5,000 25 Not Tested
2-Methylbutane (Isopentane) 750 25 Pass/<LOD 2-Methylpentane (Hexanes) 50 25 Pass/<LOD
2-Methylpropane (Isobutane) 800 25 Pass/<LOD 2-propanol (Isopropyl Alcohol) 500 25 Pass/43
2-Propanone (Acetone) 750 25 Pass/<LOD 3-Methylpentane (Hexanes) 50 25 Pass/<LOD
Acetonitrile 60 30 Pass/<LOD Benzene 1 1 Pass/<LOD
Butane 800 25 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 5,000 25 Not Tested Cyclohexane 50 25 Not Tested
Dichloromethane 125 25 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 250 Not Tested
Ethanol 1,000 50 Pass/<LOD Ethyl acetate 400 25 Pass/<LOD
Ethyl ether 500 25 Pass/<LOD Ethylene glycol 5,000 25 Not Tested
Ethylene oxide 5 3 Pass/<LOD Heptane 500 25 Pass/<LOD
Hexane 50 25 Pass/<LOD Isopropyl acetate 5,000 25 Not Tested
Methanol 250 125 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 5,000 250 Not Tested N,N-Dimethylformamide (DMF) 5,000 250 Not Tested
Pentane 750 25 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 2,100 25 Pass/<LOD Pyridine 5,000 250 Not Tested
Sulfolane 5,000 25 Not Tested Tetrahydrofuran (THF) 5,000 25 Not Tested
Toluene 150 25 Pass/<LOD Trichloroethylene 25 10 Pass/<LOD
Xylenes* 150 25 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

Total PPM: 43.00
* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information. AU License #: AU-SC-000107; MED License #: SC-000003.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 8

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Residual Solvents QC Report

Testing Accreditation #: 77802 Test Certificate #: 145844-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 2.5g PR Multipack-Pink Acai
License: AU-P-000253
Type: AU Infused Pre-Roll W/Solvents
Method: SOP FE-44-MI (GCMS)
Metrc Test Pkg#: 1A405030002A686000155310
Metrc Source Pkg#: 1A405030002A686000155209

Test Conditions

Prepsheet ID#: MIHS240304a
Scale: XS205-MI1
Temp: 22.9 °C
Baro PE: 976.9 hPa
Analyst: OSB
Technician: OSB

Sample ID#: 145844

Harvest/Process Date: 03/04/2024
Serving Size (g): 1
Date Received: 03/04/2024
Test Date: 03/04/2024
Valid Through: 03/04/2025
Report Issued: 03/05/2024

Sample #145844
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 250 254 254 101.60 101.60 0.00
n-Propane N.D. 250 198 222 79.20 88.80 11.43
Isobutane N.D. 250 232 229 92.80 91.60 1.30
Methanol N.D. 250 270 271 108.00 108.40 0.37
n-Butane N.D. 250 229 229 91.60 91.60 0.00
2,2-Dimethylpropane N.D. 250 242 240 96.80 96.00 0.83
Ethanol N.D. 250 246 255 98.40 102.00 3.59
Isopentane N.D. 250 257 247 102.80 98.80 3.97
Acetonitrile N.D. 250 225 248 90.00 99.20 9.73
Diethyl ether N.D. 250 244 242 97.60 96.80 0.82
2-propanone N.D. 250 258 244 103.20 97.60 5.58
2-propanol N.D. 250 243 249 97.20 99.60 2.44
n-Pentane N.D. 250 252 252 100.80 100.80 0.00
2,2-Dimethylbutane N.D. 250 253 253 101.20 101.20 0.00
2,3-Dimethylbutane N.D. 250 241 248 96.40 99.20 2.86
Methylene chloride N.D. 250 245 246 98.00 98.40 0.41
2-Methylpentane N.D. 250 252 251 100.80 100.40 0.40
3-Methylpentane N.D. 250 251 247 100.40 98.80 1.61
2-Butanol N.D. 0 0 0 0.00 0.00 0.00
n-Hexane N.D. 250 247 247 98.80 98.80 0.00
Ethyl acetate N.D. 250 249 250 99.60 100.00 0.40
Tetrahydrofuran N.D. 0 0 0 0.00 0.00 0.00
Trichloroethylene N.D. 250 255 251 102.00 100.40 1.58
Isopropyl acetate N.D. 0 0 0 0.00 0.00 0.00
Benzene N.D. 250 245 247 98.00 98.80 0.81
Chloroform N.D. 250 250 252 100.00 100.80 0.80
Cyclohexane N.D. 0 0 0 0.00 0.00 0.00
Ethylene glycol N.D. 0 0 0 0.00 0.00 0.00
Heptane N.D. 250 243 247 97.20 98.80 1.63
2-Ethoxyethanol N.D. 0 0 0 0.00 0.00 0.00
1,4-Dioxane N.D. 0 0 0 0.00 0.00 0.00
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 250 251 100.00 100.40 0.40
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 0 0 0 0.00 0.00 0.00
m-Xylene/p-Xylene N.D. 500 525 517 105.00 103.40 1.54
o-Xylene N.D. 250 269 266 107.60 106.40 1.12
Cumene N.D. 0 0 0 0.00 0.00 0.00
Ethylene oxide N.D. 250 200 199 80.00 79.60 0.50

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information. AU License #: AU-SC-000107; MED License #: SC-000003.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 8

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Microbiology Analysis

Testing Accreditation #: 77802 Test Certificate #: 145844-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 2.5g PR Multipack-Pink Acai
License: AU-P-000253
Type: AU Infused Pre-Roll W/Solvents
Metrc Test Pkg#: 1A405030002A686000155310
Metrc Source Pkg#: 1A405030002A686000155209

Test Conditions

Scale: Pioneer-MI1
Temp: 22.2 °C
Baro Pressure: 986.3 hPa
Analyst: EDB
Technician: EDB

Sample ID#: 145844

Harvest/Process Date: 03/04/2024
Serving Size (g): 1
Date Received: 03/04/2024
Test Date: 03/04/2024
Valid Through: 03/04/2025
Report Issued: 03/07/2024

Sample #145844
Test Method MCFU (CFU/g) LOD (CFU/g) Status (CFU/g)
Total Aerobic Not Tested N/A 0 Not Tested
Yeast & Mold FE-66 (MPN) 100,001 100 Pass/<LOD
Bile-tolerant gram-negative bacteria Not Tested N/A 0 Not Tested
Total Coliforms FE-66 (MPN) 1,001 100 Pass/<LOD
E. Coli FE-65 (PCR) 1 1 Pass/Not Present
Salmonella FE-65 (PCR) 1 1 Pass/Not Present
Aspergillus spp. FE-65 (PCR) 1 1 Pass/Not Present

E. coli test screens exclusively for Shiga toxin-producing E. coli. TNTC values for yeast and mold are >150,000 CFU/g. TNTC values for total coliforms are >15,000 CFU/g. The maximum relative uncertainty is 6% for PCR and 40% for MPN.

TNTC = Too Numerous To Count. Maximum Colony Forming Units (MCFU) represents the minimum value that a test would need to achieve in order to be considered a failed result (if applicable). LOD is the Limit of Detection for the method. CFU/g = Colony Forming Units per gram. Aspergillus spp. consists of A. flavus, A. fumigatus, A. niger, and A. terreus.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information. AU License #: AU-SC-000107; MED License #: SC-000003.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 6 of 8

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Bio Analysis by
Microscopic Visual Inspection

Testing Accreditation #: 77802 Test Certificate #: 145844-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 2.5g PR Multipack-Pink Acai
License: AU-P-000253
Type: AU Infused Pre-Roll W/Solvents
Method: FE02 Microscope Dissection
Metrc Test Pkg#: 1A405030002A686000155310
Metrc Source Pkg#: 1A405030002A686000155209

Test Conditions

Analyst: ARH
Technician: ARH

Sample ID#: 145844

Harvest/Process Date: 03/04/2024
Serving Size (g): 1
Date Received: 03/04/2024
Test Date: 03/04/2024
Valid Through: 03/04/2025
Report Issued: 03/04/2024

Sample #145844
Sample #145844 Sample #145844
Severity Rating
Mold and Mildew 0 Pass
Mites (not Russet) 0 Pass
Russet Mites 0 Pass
Thrips 0 Pass
Aphids 0 Pass
Other Pests 0 Pass
Other Organic Matter 0 Pass
Inorganic Matter 0 Pass
Total Organic Foreign Matter <2% Pass
Inorganic Foreign Matter 0% Pass
Stem Material <5% Pass
Severity Rating Key
Correlating %FM ≤2% FM >2% FM
Severity Rating 0 None 1 Mild 2 Moderate 3 Severe Units
Mold and Mildew <2 2 3 4+ Locations/g
Mites (not russet) <1 1-5 6-10 11+ Amount/g
Russet Mites <1 1-10 11-50 51+ Amount/g
Thrips <1 1-3 4-5 6+ Amount/g
Aphids <1 1 2-4 5+ Amount/g
Other Pests <1 1-5 6-10 11+ Amount/g
Other Organic Matter <1 1-5 6-10 11+ Amount/g
Inorganic Matter 0 >0 Amount/g

In compliance with the MMFLA regulation, the action limits for foreign matter are as follows; no more that 2% organic matter, 5% stem material, and no presence of inorganic matter. Percent foreign contamination is based off of total surface area.

Scale: PIONEER-MI1.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information. AU License #: AU-SC-000107; MED License #: SC-000003.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 7 of 8

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Heavy Metals Analysis

Testing Accreditation #: 77802 Test Certificate #: 145844-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 2.5g PR Multipack-Pink Acai
License: AU-P-000253
Type: AU Infused Pre-Roll W/Solvents
Method: FE60 ICPMS
Metrc Test Pkg#: 1A405030002A686000155310
Metrc Source Pkg#: 1A405030002A686000155209

Test Conditions

Prepsheet ID#: HMMIICP240304cMK
Temp: 23.0 °C
Baro PE: 979.9 hPa
Analyst: MK
Technician: MK

Sample ID#: 145844

Harvest/Process Date: 03/04/2024
Serving Size (g): 1
Date Received: 03/04/2024
Test Date: 03/04/2024
Valid Through: 03/04/2025
Report Issued: 03/04/2024

Sample #145844
Sample #145844 Sample #145844
Test Compound MRL (PPM) LOD (PPM) Status (PPM)
Arsenic 0.2 0.1 Pass/<LOD
Copper 0 1.5 Not Tested
Cadmium 0.2 0.1 Pass/<LOD
Chromium 0.6 0.3 Pass/<LOD
Lead 0.5 0.25 Pass/<LOD
Mercury 0.1 0.05 Pass/<LOD
Nickel 0.5 0.25 Pass/<LOD

MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information. AU License #: AU-SC-000107; MED License #: SC-000003.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 8 of 8

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 145844-001
Client Name, Sample Details

Ferndale Maize LLC - STIIIZY (AU-P-000253)
Lake Orion, MI 48359
Sample: Stiiizy 2.5g PR Multipack-Pink Acai
License: AU-P-000253
Type: AU Infused Pre-Roll W/Solvents
Method: FE60 ICPMS
Metrc Test Pkg#: 1A405030002A686000155310
Metrc Source Pkg#: 1A405030002A686000155209

Test Conditions

Prepsheet ID#: HMMIICP240304cMK
Temp: 23.0 °C
Baro PE: 979.9 hPa
Analyst: MK
Technician: MK

Sample ID#: 145844

Harvest/Process Date: 03/04/2024
Serving Size (g): 1
Date Received: 03/04/2024
Test Date: 03/04/2024
Valid Through: 03/04/2025
Report Issued: 03/04/2024

Sample #145844
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD QC Flag
Arsenic N/D 0.160 0.161 100.63 0.155 96.88
Cadmium N/D 0.160 0.150 93.75 0.141 88.13
Chromium N/D 0.480 0.435 90.63 0.435 90.63
Copper N/D 2.400 1.912 79.67 1.967 81.96
Lead N/D 0.400 0.374 93.50 0.370 92.50
Mercury N/D 0.080 0.084 105.00 0.082 102.50
Nickel N/D 0.400 0.394 98.50 0.383 95.75

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information. AU License #: AU-SC-000107; MED License #: SC-000003.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 9 of 8