IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 130427-001
Client Name, Sample Details

Taboo Treasures
Detroit , MI 48228
Sample: Salve
License: CG-20-036894
Type: Topical
Method: FE04U HPLC-UV

Test Conditions

Prepsheet ID#: MIP210420a
Scale: XS205-MI2
Temp: 21.6 °C
Baro Pressure: 970.3 hPa
Analyst: KEB
Technician: VU/KEB

Sample ID#: 130427

Harvest/Process Date: 04/21/2021
Serving Size (g): 46.11
Date Received: 04/21/2021
Test Date: 04/20/2021
Valid Through: 04/21/2022
Report Issued: 04/21/2021

Sample #130427
Sample #130427 Sample #130427
Test
Compounds
THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.0 N/D 1.9 0.0 N/D 0.0 N/D N/D 0.0 1.9 0.0 1.9 1.9
Amount (mg/g) 0.2 N/D 18.9 0.1 N/D 0.1 N/D N/D 0.1 19.4 0.2 19.0 19.4
Amount per Serving (mg) 9.2 N\D 871.5 4.6 N\D 4.6 N\D N\D 4.6 894.5 Serving Size~ (g): 46.1
LOQ (mg/g) 0.07 0.07 0.07 0.07 0.07 0.07 0.07 0.07 0.07   %Decarb. THC CBD
±%RPD 1.48 1.80 1.80 0.28 0.71 0.91 1.26 0.11 0.84 100% 99

1 pkg= 46.11073g; Target= 250 mg CBD/pkg

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 130427-001
Client Name, Sample Details

Taboo Treasures
Detroit , MI 48228
Sample: Salve
License: CG-20-036894
Type: Topical
Method: FE04U HPLC-UV

Test Conditions

Prepsheet ID#: MIP210420a
Scale: XS205-MI2
Temp: 21.6 °C
Baro Pressure: 970.3 hPa
Analyst: KEB
Technician: VU/KEB

Sample ID#: 130427

Harvest/Process Date: 04/21/2021
Serving Size (g): 46.11
Date Received: 04/21/2021
Test Date: 04/20/2021
Valid Through: 04/21/2022
Report Issued: 04/21/2021

Sample #130427
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 5.51483917 5.602417661 101.59 5.649552527 102.44 0.84
Cannabidiolic Acid (CBDA) 0 5.627477053 5.68820163 101.08 5.704359387 101.37 0.28
Cannabigerol (CBG) 0 5.593118766 5.713230204 102.15 5.765263752 103.08 0.91
Cannabidiol (CBD) 0 5.567611848 5.600571199 100.59 5.702265695 102.42 1.80
Δ9-Tetrahydrocannabivarin (THCV) 0 5.924721405 6.022778755 101.66 6.029695745 101.77 0.11
Cannabinol (CBN) 0 5.431501118 5.511294592 101.47 5.550588475 102.19 0.71
Δ9-Tetrahydrocannabinol (THC) 0 5.241331072 5.341027744 101.90 5.420916461 103.43 1.48
Cannabichromene (CBC) 0 5.497268936 5.716496283 103.99 5.789105399 105.31 1.26
Tetrahydrocannabinolic acid (THCA) 0 5.283260329 5.448810099 103.13 5.547979268 105.01 1.80

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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