ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-004 Test Certificate #: 126107-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Holy Grail
License: 010-100164183CE
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300017891000000542
Metrc Source Pkg#: 1A4010300017891000000531
***Water Activity: 0.571
***Moisture: 12.89%
Test Conditions

Prepsheet ID#: ORP200824a
Scale: XS205-OR1
Temp: 21.6 °C
Baro Pressure: 1005 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 126107

Lot #: Holy Grail 8/5/20
Batch #: 126107
Batch Weight (g): 6810
Harvest/Process Date: 08/05/2020
Date Received: 08/20/2020
Test Date: 08/24/2020
Sample #126107
Sample #126107 Sample #126107
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.94 21.21 N/D 0.44 0.11 0.18 0.08 N/D N/D 22.96 19.54 0.38 20.30
Amount (mg/g) 9.35 212.11 N/D 4.38 1.11 1.81 0.83 N/D N/D 229.59 195.37 3.84 202.96
Amount per Serving (mg) N\D N\D N\D N\D N\D N\D N\D N\D N\D 0.00 Serving Size~ (g): 0.00
LOQ (mg/g) 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5   %Decarb. THC CBD
±%RPD +/-5% 9.31 +/-5% 13.13 8.33 2.54 5.00 +/-5% +/-5% 4 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 126107-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Holy Grail
License: 010-100164183CE
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300017891000000542
Metrc Source Pkg#: 1A4010300017891000000531
***Water Activity: 0.571
***Moisture: 12.89%
Test Conditions

Prepsheet ID#: ORP200824a
Scale: XS205-OR1
Temp: 21.6 °C
Baro Pressure: 1005 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 126107

Lot #: Holy Grail 8/5/20
Batch #: 126107
Batch Weight (g): 6810
Harvest/Process Date: 08/05/2020
Date Received: 08/20/2020
Test Date: 08/24/2020
Sample #126107
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 1 0 0.00 0 0.00 0
Cannabidiolic Acid (CBDA) N.D. 11.33 11.12 98.15 9.75 86.05 13.13
Cannabigerol (CBG) N.D. 1.78 1.99 111.80 1.94 108.99 2.54
Cannabidiol (CBD) N.D. 1 0 0.00 0 0.00 0
Δ9-Tetrahydrocannabivarin (THCV) N.D. 1 0 0.00 0 0.00 0
Cannabinol (CBN) N.D. 0.42 0.69 164.29 0.75 178.57 8.33 HR
Δ9-Tetrahydrocannabinol (THC) 1 0.00 0.00 0
Cannabichromene (CBC) N.D. 0.64 0.82 128.13 0.78 121.88 5.00
Tetrahydrocannabinolic acid (THCA) N.D. 150.95 145.87 96.63 132.89 88.04 9.31

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 126107-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Holy Grail
License: 010-100164183CE
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300017891000000542
Metrc Source Pkg#: 1A4010300017891000000531

Test Conditions

Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1001.2 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 126107

Lot #: Holy Grail 8/5/20
Batch #: 126107
Batch Weight (g): 6810
Harvest/Process Date: 08/05/2020
Date Received: 08/20/2020

Sample #126107
Sample #126107
  • α-Pinene (0.00%)
  • β-Ocimene (0.05%)
  • Camphene (0.00%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.00%)
  • Myrcene (0.24%)
  • α-Terpinolene (0.00%)
  • β-Pinene (0.29%)
  • Linalool (0.23%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.00%)
  • endo-Fenchol (0.04%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.14%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.00%)
  • α-Humulene (0.29%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.02%)
  • Guaiol (0.16%)
  • Caryophyllene Oxide (0.00%)
  • α-Bisabolol (0.05%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.09%)
  • Valenence (0.36%)

Total: 1.960%

Predominant Terpenes

0.36%   Valenence Sweet, citrus, grapefruit, woody, orange 0.29%   α-Humulene Woody, oceanic-watery, spicy clove
0.29%   β-Pinene Woody, fresh pine, hay 0.24%   Myrcene Peppery, spicy balsam
0.23%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry 0.16%   Guaiol Mild, guaiacwood, tea, rose

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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