ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 119623-001
Client Name, Sample Details

The Dankside
Alsea, OR 97324
Sample: Wedding Cake
License: 020-10035593CF8
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300009FC6000000745
Metrc Source Pkg#: 1A4010300009FC6000000736
***Water Activity: 0.5246
***Moisture: 13.4%
Test Conditions

Prepsheet ID#: ORP191023a
Scale: XS205-OR1
Temp: 23.6 °C
Baro Pressure: 1008 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 119623

Lot #: wedding cake 9/6/2019
Batch #: 119623
Batch Weight (g): 1386
Harvest/Process Date: 09/06/2019
Serving Size (g): 1
Date Received: 10/15/2019
Test Date: 10/23/2019
Sample #119623
Sample #119623 Sample #119623
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 2.41 29.94 N/D 1.16 0.11 0.09 N/D N/D N/D 33.69 28.66 1.02 29.87
Amount (mg/g) 24.07 299.36 N/D 11.59 1.06 0.85 N/D N/D N/D 336.93 286.61 10.16 298.68
Amount per Serving (mg) 24.07 299.36 N\D 11.59 1.06 0.85 N\D N\D N\D 336.93 Serving Size~ (g): 1.00
LOQ (mg/g) 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05   %Decarb. THC CBD
±%RPD 0.58 0.27 +/-5% 2.09 15.38 10.53 +/-5% +/-5% +/-5% 7 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 2

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 119623-001
Client Name, Sample Details

The Dankside
Alsea, OR 97324
Sample: Wedding Cake
License: 020-10035593CF8
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300009FC6000000745
Metrc Source Pkg#: 1A4010300009FC6000000736
***Water Activity: 0.5246
***Moisture: 13.4%
Test Conditions

Prepsheet ID#: ORP191023a
Scale: XS205-OR1
Temp: 23.6 °C
Baro Pressure: 1008 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 119623

Lot #: wedding cake 9/6/2019
Batch #: 119623
Batch Weight (g): 1386
Harvest/Process Date: 09/06/2019
Serving Size (g): 1
Date Received: 10/15/2019
Test Date: 10/23/2019
Sample #119623
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 1 0 0.00 0 0.00 0
Cannabidiolic Acid (CBDA) N.D. 1.29 1.45 112.40 1.42 110.08 2.09
Cannabigerol (CBG) N.D. 0.16 0.2 125.00 0.18 112.50 10.53
Cannabidiol (CBD) N.D. 1 0 0.00 0 0.00 0
Δ9-Tetrahydrocannabivarin (THCV) N.D. 1 0 0.00 0 0.00 0
Cannabinol (CBN) N.D. 0.1 0.07 70.00 0.06 60.00 15.38
Δ9-Tetrahydrocannabinol (THC) N.D. 3.31 3.43 103.63 3.41 103.02 0.58
Cannabichromene (CBC) N.D. 0.08 0.13 162.50 0.13 162.50 0.00
Tetrahydrocannabinolic acid (THCA) N.D. 18.31 18.75 102.40 18.7 102.13 0.27

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 2
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 119623-001
Client Name, Sample Details

The Dankside
Alsea, OR 97324
Sample: Wedding Cake
License: 020-10035593CF8
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300009FC6000000745
Metrc Source Pkg#: 1A4010300009FC6000000736

Test Conditions

Scale: XS205-OR1
Temp: 21.2 °C
Baro Pressure: 999.8 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 119623

Lot #: wedding cake 9/6/2019
Batch #: 119623
Batch Weight (g): 1386
Harvest/Process Date: 09/06/2019
Serving Size (g): 1
Date Received: 10/15/2019

Sample #119623
Sample #119623
  • α-Pinene (0.05%)
  • β-Ocimene (0.00%)
  • Camphene (0.02%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.00%)
  • Myrcene (0.27%)
  • α-Terpinolene (0.03%)
  • β-Pinene (0.09%)
  • Linalool (0.14%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.00%)
  • endo-Fenchol (0.09%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.22%)
  • Geraniol (0.01%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.50%)
  • α-Humulene (0.21%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.00%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.00%)
  • α-Bisabolol (0.03%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.07%)
  • Valenence (0.22%)

Total: 1.950%

Predominant Terpenes

0.50%   β-Caryophyllene Sweet, woody, spicy, clove 0.27%   Myrcene Peppery, spicy balsam
0.22%   Valenence Sweet, citrus, grapefruit, woody, orange 0.22%   Limonene Citrus, orange, sweet
0.21%   α-Humulene Woody, oceanic-watery, spicy clove 0.14%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 2