IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 118949-001
Client Name, Sample Details

Holistic Healing Tim/RoseAnn
Troy, MI 48083
Sample: 3000 mg Broad MCT
Type: Tincture
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP190814
Scale: XS205-MI2
Temp: 22.1 °C
Baro Pressure: 978.6 hPa
Analyst: KEB
Technician: KEB
Sample ID#: 118949

Harvest/Process Date: 08/15/2019
Serving Size (g): 0.92
Date Received: 08/15/2019
Test Date: 08/14/2019
Valid Through: 08/14/2020
Report Issued: 08/15/2019
Sample #118949
Sample #118949 Sample #118949
Test
Compounds		 THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) N/D N/D 14.7 0.1 0.2 N/D 0.4 N/D 0.2 15.5 0.0 14.8 15.5
Amount (mg/g) N/D N/D 146.7 1.2 1.9 N/D 3.5 N/D 1.5 154.8 0.0 147.8 154.7
Amount per Serving (mg) N\D N\D 135.0 1.1 1.7 N\D 3.2 N\D 1.4 142.4 Serving Size~ (g): 0.9
LOQ (mg/g) 0.97 0.97 0.97 0.97 0.97 0.97 0.97 0.97 0.97   %Decarb. THC CBD
±%RPD 1.87 2.30 2.09 2.48 1.20 2.42 0.61 1.63 1.63 N/A 99

Serving size = 1 mL

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 118949-001
Client Name, Sample Details

Holistic Healing Tim/RoseAnn
Troy, MI 48083
Sample: 3000 mg Broad MCT
Type: Tincture
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP190814
Scale: XS205-MI2
Temp: 22.1 °C
Baro Pressure: 978.6 hPa
Analyst: KEB
Technician: KEB
Sample ID#: 118949

Harvest/Process Date: 08/15/2019
Serving Size (g): 0.92
Date Received: 08/15/2019
Test Date: 08/14/2019
Valid Through: 08/14/2020
Report Issued: 08/15/2019
Sample #118949
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 4.8433 4.79749 99.05 4.87614 100.68 1.63
Cannabidiolic Acid (CBDA) 0 4.7643 4.81037 100.97 4.93114 103.50 2.48
Cannabigerol (CBG) 0 4.78775 4.8707 101.73 4.99013 104.23 2.42
Cannabidiol (CBD) 0 4.25219 4.27645 100.57 4.36699 102.70 2.09
Δ9-Tetrahydrocannabivarin (THCV) 0 4.67328 4.7041 100.66 4.78151 102.32 1.63
Cannabinol (CBN) 0 4.70271 4.7724 101.48 4.82979 102.70 1.20
Δ9-Tetrahydrocannabinol (THC) 0 5.11708 5.57001 108.85 5.4666 106.83 1.87
Cannabichromene (CBC) 0 5.39412 5.65678 104.87 5.62214 104.23 0.61
Tetrahydrocannabinolic acid (THCA) 0 4.92792 5.37218 109.02 5.25002 106.54 2.30

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 1