ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-002 Test Certificate #: 117011-001
Client Name, Sample Details

45th Parallel Farms #2
Dallas, OR 97338
Sample: Mixed batch pest 117009 - 117010
License: 100861828BC
Type: Usable Marijuana
Method: FE-52 (EN 15662 & AOAC 2007.01)

Test Conditions

Prepsheet ID#: ORPS190521a
Scale: Veritas-OR1
Temp: 21.5 °C
Baro PE: 991.1 hPa
Analyst: JDM
Technician: JDM

Sample ID#: 117011

Batch #: 117011
Batch Weight (g): 5846.8
Harvest/Process Date: 05/17/2019
Date Received: 05/17/2019
Test Date: 05/23/2019

Sample #117011
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.120 Pass/<LOD Abamectin**** 0.500 0.120 Pass/<LOD
Acephate 0.400 0.120 Pass/<LOD Acequinocyl 2.000 0.240 Pass/<LOD
Acetamiprid 0.200 0.120 Pass/<LOD Azoxystrobin 0.200 0.120 Pass/<LOD
Bifenazate 0.200 0.120 Pass/<LOD Bifenthrin 0.200 0.120 Pass/<LOD
Boscalid 0.400 0.120 Pass/<LOD Carbaryl 0.200 0.120 Pass/<LOD
Carbofuran 0.200 0.120 Pass/<LOD Chlorantraniliprole 0.200 0.120 Pass/<LOD
Chlorfenapyr 1.000 0.481 Pass/<LOD Chlorpyrifos 0.200 0.120 Pass/<LOD
Clofentezine 0.200 0.120 Pass/<LOD Cyfluthrin** 1.000 0.481 Pass/<LOD
Cypermethrin*** 1.000 0.481 Pass/<LOD Daminozide 1.000 0.120 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.240 Pass/<LOD Diazinon 0.200 0.120 Pass/<LOD
Dimethoate 0.200 0.120 Pass/<LOD Ethoprophos 0.200 0.120 Pass/<LOD
Etofenprox 0.400 0.120 Pass/<LOD Etoxazole 0.200 0.120 Pass/<LOD
Fenoxycarb 0.200 0.120 Pass/<LOD Fenpyroximate 0.400 0.120 Pass/<LOD
Fipronil 0.400 0.120 Pass/<LOD Flonicamid 1.000 0.120 Pass/<LOD
Fludioxonil 0.400 0.120 Pass/<LOD Hexythiazox 1.000 0.120 Pass/<LOD
Imazalil 0.200 0.120 Pass/<LOD Imidacloprid 0.400 0.120 Pass/<LOD
Kresoxim Methyl 0.400 0.120 Pass/<LOD Malathion 0.200 0.120 Pass/<LOD
Metalaxyl 0.200 0.120 Pass/<LOD Methiocarb 0.200 0.120 Pass/<LOD
Methomyl 0.400 0.120 Pass/<LOD Methyl Parathion 0.200 0.120 Pass/<LOD
MGK-264‡ 0.200 0.120 Pass/<LOD Myclobutanil 0.000 0.120 Pass/<LOD
Naled 0.500 0.120 Pass/<LOD Oxamyl 1.000 0.120 Pass/<LOD
Paclobutrazol 0.400 0.120 Pass/<LOD Permethrins† 0.200 0.120 Pass/<LOD
Phosmet 0.200 0.120 Pass/<LOD Piperonyl Butoxide 2.000 0.120 Pass/<LOD
Prallethrin 0.200 0.120 Pass/<LOD Propiconazole 0.400 0.120 Pass/<LOD
Propoxur 0.200 0.120 Pass/<LOD Pyrethrins* 1.000 0.120 Pass/<LOD
Pyridaben 0.200 0.120 Pass/<LOD Spinosad***** 0.200 0.120 Pass/<LOD
Spiromesifen 0.200 0.120 Pass/<LOD Spirotetramat 0.200 0.120 Pass/<LOD
Spiroxamine‡ 0.400 0.120 Pass/<LOD Tebuconazole 0.400 0.120 Pass/<LOD
Thiacloprid 0.200 0.120 Pass/<LOD Thiamethoxam 0.200 0.120 Pass/<LOD
Trifloxystrobin 0.200 0.120 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report

Testing Accreditation #: 4092-002 Test Certificate #: 117011-001
Client Name, Sample Details

45th Parallel Farms #2
Dallas, OR 97338
Sample: Mixed batch pest 117009 - 117010
License: 100861828BC
Type: Usable Marijuana
Method: FE-52 (EN 15662 & AOAC 2007.01)

Test Conditions

Prepsheet ID#: ORPS190521a
Scale: Veritas-OR1
Temp: 21.5 °C
Baro PE: 991.1 hPa
Analyst: JDM
Technician: JDM

Sample ID#: 117011

Batch #: 117011
Batch Weight (g): 5846.8
Harvest/Process Date: 05/17/2019
Date Received: 05/17/2019
Test Date: 05/23/2019

Sample #117011
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.25 1.36 125.00 136.00 8.43 HR
Acequinocyl N.D. 1 0.722 0.589 72.20 58.90 20.29 Q
Acetamiprid N.D. 1 1.35 1.36 135.00 136.00 0.74 HR
Aldicarb N.D. 1 1.31 1.36 131.00 136.00 3.75 Q
Avermectin B1a N.D. 0.97 1.76 1.21 181.44 124.74 37.04 HR
Azoxystrobin N.D. 1 1.43 1.51 143.00 151.00 5.44 HR
Bifenazate N.D. 1 1.34 1.43 134.00 143.00 6.50 HR
Bifenthrin N.D. 1 1.38 1.4 138.00 140.00 1.44 HR
Boscalid N.D. 1 1.25 1.33 125.00 133.00 6.20 HR
Carbaryl N.D. 1 1.35 1.19 135.00 119.00 12.60 HR
Carbofuran N.D. 1 1.52 1.53 152.00 153.00 0.66 HR
Chlorantraniliprole N.D. 1 1.55 1.78 155.00 178.00 13.81 HRQ
Chlorfenapyr N.D. 1 1.19 1.59 119.00 159.00 28.78 HR
Chlorpyriphos N.D. 1 1.28 1.33 128.00 133.00 3.83 HR
Clofentezine N.D. 1 1.22 1.27 122.00 127.00 4.02
Cyfluthrin N.D. 1 1.76 1.51 176.00 151.00 15.29 HR
Cypermethrin N.D. 1 1.63 1.62 163.00 162.00 0.62 HR
Daminoside N.D. 1 0.489 0.482 48.90 48.20 1.44 LR
Diazanon N.D. 1 1.44 1.55 144.00 155.00 7.36 HR
Dichlorvos N.D. 1 1.53 1.69 153.00 169.00 9.94 HR
Dimethoate N.D. 1 1.4 1.43 140.00 143.00 2.12 HR
Ethoprophos N.D. 1 1.42 1.5 142.00 150.00 5.48 HR
Etofenprox N.D. 1 1.33 1.39 133.00 139.00 4.41 HR
Etoxazole N.D. 1 1.49 1.3 149.00 130.00 13.62 HR
Fenoxycarb N.D. 1 1.54 1.65 154.00 165.00 6.90 HR
Fenpyroximate N.D. 1 1.48 1.5 148.00 150.00 1.34 HR
Fipronil N.D. 1 1.31 1.23 131.00 123.00 6.30 HR
Flonicamid N.D. 1 1.55 1.51 155.00 151.00 2.61 HR
Fludioxonil N.D. 1 1.34 1.32 134.00 132.00 1.50 HR
Hexythiazox N.D. 1 1.37 1.33 137.00 133.00 2.96 HR
Imazalil N.D. 1 1.51 1.58 151.00 158.00 4.53 HR
Imidacloprid N.D. 1 1.55 1.68 155.00 168.00 8.05 HR
Kresoxim-methyl N.D. 1 1.32 1.58 132.00 158.00 17.93 HR
Malathion N.D. 1 1.28 1.34 128.00 134.00 4.58 HR
Metalaxyl N.D. 1 1.56 1.73 156.00 173.00 10.33 HR
Methiocarb N.D. 1 1.44 1.49 144.00 149.00 3.41 HR
Methomyl N.D. 1 1.43 1.41 143.00 141.00 1.41 HR
MGK-264 N.D. 1 1.47 1.41 147.00 141.00 4.17 HR
Myclobutanil N.D. 1 1.61 1.66 161.00 166.00 3.06 HR
Naled (dibrom) N.D. 1 0.78 0.828 78.00 82.80 5.97
Oxamyl N.D. 1 1.57 1.64 157.00 164.00 4.36 HR
Paclobutrazol N.D. 1 1.51 1.61 151.00 161.00 6.41 HR
Parathion-methyl N.D. 1 1.21 1.22 121.00 122.00 0.82
Permethrins N.D. 1 1.39 1.48 139.00 148.00 6.27 HR
Phosmet N.D. 1 1.37 1.4 137.00 140.00 2.17 HR
Piperonyl butoxide N.D. 1 1.34 1.33 134.00 133.00 0.75 HR
Prallethrin N.D. 1 1.44 1.55 144.00 155.00 7.36 HR
Propiconazole N.D. 1 1.25 1.31 125.00 131.00 4.69 HR
Propoxur N.D. 1 1.29 1.49 129.00 149.00 14.39 HR
Pyrethrin N.D. 0.65 0.748 0.724 115.08 111.38 3.26
Pyridaben N.D. 1 1.25 1.22 125.00 122.00 2.43
SpinosynA N.D. 0.84 1.5 1.62 178.57 192.86 7.69 HR
SpinosynD N.D. 0.16 0.333 0.35 208.13 218.75 4.98 HR
Spiromesifen N.D. 1 0.0968 0.0963 9.68 9.63 0.52
Spirotetramat N.D. 1 0.844 0.907 84.40 90.70 7.20
Spiroxamine N.D. 1 1.65 1.74 165.00 174.00 5.31 HR
Tebuconazole N.D. 1 1.45 1.52 145.00 152.00 4.71 HR
Thiacloprid N.D. 1 1.58 1.65 158.00 165.00 4.33 HR
Thiamethoxam N.D. 1 1.55 1.55 155.00 155.00 0.00 HR
Trifloxystrobin N.D. 1 1.34 1.36 134.00 136.00 1.48 HR

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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