IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 114911-001
Client Name, Sample Details

John Kassa
Wixom, MI 48393
Sample: Lime Skunk #1
Type: Flower
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP190207
Scale: XS205-MI2
Temp: 21.3 °C
Baro Pressure: 987 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 114911

Harvest/Process Date: 02/08/2019
Serving Size (g): 1
Date Received: 02/08/2019
Test Date: 02/08/2019
Valid Through: 02/08/2020
Report Issued: 02/11/2019
Sample #114911
Sample #114911 Sample #114911
Test
Compounds		 THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.9 28.1 N/D 1.5 0.1 0.2 N/D N/D N/D 30.9 25.6 1.3 27.2
Amount (mg/g) 9.0 281.1 N/D 14.9 1.3 2.3 N/D N/D N/D 308.6 255.5 13.0 272.1
Amount per Serving (mg) 9.0 281.1 N\D 14.9 1.3 2.3 N\D N\D N\D 308.6 Serving Size~ (g): 1.0
LOQ (mg/g) 0.99 0.99 0.99 0.99 0.99 0.99 0.99 0.99 0.99   %Decarb. THC CBD
±%RPD 2.68 2.49 0.38 5.61 0.91 0.86 7.21 2.82 0.07 3 0%

Results not adjusted for moisture.

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 3

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 114911-001
Client Name, Sample Details

John Kassa
Wixom, MI 48393
Sample: Lime Skunk #1
Type: Flower
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP190207
Scale: XS205-MI2
Temp: 21.3 °C
Baro Pressure: 987 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 114911

Harvest/Process Date: 02/08/2019
Serving Size (g): 1
Date Received: 02/08/2019
Test Date: 02/08/2019
Valid Through: 02/08/2020
Report Issued: 02/11/2019
Sample #114911
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 1.94863 2.08275 106.88 2.08136 106.81 0.07
Cannabidiolic Acid (CBDA) 0 5.40387 5.40014 99.93 5.71202 105.70 5.61
Cannabigerol (CBG) 0 4.04311 4.13688 102.32 4.17241 103.20 0.86
Cannabidiol (CBD) 0 5.61397 5.73602 102.17 5.75778 102.56 0.38
Δ9-Tetrahydrocannabivarin (THCV) 0 2.71337 2.79034 102.84 2.87018 105.78 2.82
Cannabinol (CBN) 0 5.14456 5.18451 100.78 5.23189 101.70 0.91
Δ9-Tetrahydrocannabinol (THC) 0 6.80012 6.86876 101.01 7.05564 103.76 2.68
Cannabichromene (CBC) 0 6.08638 6.38773 104.95 6.86541 112.80 7.21
Tetrahydrocannabinolic acid (THCA) 0 5.80123 6.1117 105.35 5.96161 102.76 2.49

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 3
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 114911-001
Client Name, Sample Details

John Kassa
Wixom, MI 48393
Sample: Lime Skunk #1
Type: Flower
Method: SOP FE-44-OR3
Test Conditions

Scale: XS205-MI1
Temp: 21.7 °C
Baro Pressure: 962.4 hPa
Analyst: MEH
Technician: JRT
Sample ID#: 114911

Harvest/Process Date: 02/08/2019
Serving Size (g): 1
Date Received: 02/08/2019
Test Date: 02/12/2019
Valid Through: 02/12/2020
Report Issued: 02/13/2019
Sample #114911

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.240 %

β-Ocimene:

0.080 %

Camphene:

0.020 %

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

0.290 %

α-Terpinolene:

0.030 %

β-Pinene:

0.160 %

Linalool:

0.050 %

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

0.080 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.800 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.280 %

α-Humulene:

0.100 %

Nerolidol 1:

 N/D

Nerolidol 2:

0.030 %

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

0.020 %

Other Terpenes

Total: 2.180%
a-Phellandrene = 0.00 % a-Terpineol = 0.06 % Valencene = 0.00 % (Other terpenes are not included in the total)

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 3

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Bio Analysis by
Microscopic Visual Inspection
Testing Accreditation #: 77802 Test Certificate #: 114911-001
Client Name, Sample Details

John Kassa
Wixom, MI 48393
Sample: Lime Skunk #1
Type: Flower
Method: FE02 Microscope Dissection
Test Conditions

Analyst: ACR
Technician: SEB
Sample ID#: 114911

Harvest/Process Date: 02/08/2019
Serving Size (g): 1
Date Received: 02/08/2019
Test Date: 02/15/2019
Valid Through: 02/15/2020
Report Issued: 02/15/2019
Sample #114911
Sample #114911 Sample #114911
Impurities: Not Detected
Molds: No Types: N/A
Pests: No Types: N/A
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture 6

The gland heads range from small to large in size and are moderately abundant. Slightly more of them are clear than milky with a moderate amount turning amber in color. Some of the trichomes are damaged and degrading. A few of the trichomes are reduced due to stress. Less than 2% foreign matter. Less than 5% stem material. If you are interested in additional testing for quantitative microbial results, please call the lab within a 1-2 days to add on additional testing.

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 3