IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 114899-001
Client Name, Sample Details

Secrets of Hemp
Columbus , IN 47201
Sample: Big Buddah Flower
Type: Flower
Method: FE04U HPLC-UV
***Moisture: 13.02%

Test Conditions

Prepsheet ID#: MIP190207
Scale: XS205-MI2
Temp: 21.2 °C
Baro Pressure: 972.5 hPa
Analyst: JRT
Technician: JRT

Sample ID#: 114899

Harvest/Process Date: 02/07/2019
Serving Size (g): 1
Date Received: 02/07/2019
Test Date: 02/07/2019
Valid Through: 02/07/2020
Report Issued: 02/08/2019

Sample #114899
Sample #114899 Sample #114899
Test
Compounds
THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.1 0.6 1.0 18.3 N/D N/D N/D N/D N/D 20.0 0.7 17.0 17.7
Amount (mg/g) 1.2 6.3 10.1 182.6 N/D N/D N/D N/D N/D 200.2 6.7 170.2 177.0
Amount per Serving (mg) 1.2 6.3 10.1 182.6 N\D N\D N\D N\D N\D 200.2 Serving Size~ (g): 1.0
LOQ (mg/g) 0.99 0.99 0.99 0.99 0.99 0.99 0.99 0.99 0.99   %Decarb. THC CBD
±%RPD 4.35 5.55 1.44 0.26 0.91 1.51 27.25 3.51 2.06 16 5

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 114899-001
Client Name, Sample Details

Secrets of Hemp
Columbus , IN 47201
Sample: Big Buddah Flower
Type: Flower
Method: FE04U HPLC-UV
***Moisture: 13.02%

Test Conditions

Prepsheet ID#: MIP190207
Scale: XS205-MI2
Temp: 21.2 °C
Baro Pressure: 972.5 hPa
Analyst: JRT
Technician: JRT

Sample ID#: 114899

Harvest/Process Date: 02/07/2019
Serving Size (g): 1
Date Received: 02/07/2019
Test Date: 02/07/2019
Valid Through: 02/07/2020
Report Issued: 02/08/2019

Sample #114899
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 2.10524 2.18137 103.62 2.22686 105.78 2.06
Cannabidiolic Acid (CBDA) 0 5.54975 5.70547 102.81 5.72048 103.08 0.26
Cannabigerol (CBG) 0 4.12746 4.32448 104.77 4.25958 103.20 1.51
Cannabidiol (CBD) 0 5.59965 5.76437 102.94 5.84777 104.43 1.44
Δ9-Tetrahydrocannabivarin (THCV) 0 2.62587 2.84666 108.41 2.9483 112.28 3.51
Cannabinol (CBN) 0 5.10604 5.3163 104.12 5.26808 103.17 0.91
Δ9-Tetrahydrocannabinol (THC) 0 6.10362 7.07789 115.96 6.77642 111.02 4.35
Cannabichromene (CBC) 0 5.6014 6.85459 122.37 5.21062 93.02 27.25
Tetrahydrocannabinolic acid (THCA) 0 5.56835 6.10048 109.56 6.4486 115.81 5.55

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 1