IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 112339-001
Client Name, Sample Details

Mitten Maid
Lansing, MI 48910
Sample: Yumbolt Nug Run Live Resin Badder
Type: Undiluted
Method: FE04P HPLC1100-1

Test Conditions

Scale: XS205-MI1
Temp: 20.7 °C
Baro Pressure: 979.5 hPa
Analyst: MEH
Technician: ACR

Sample ID#: 112339

Harvest Date: 10/15/2018
Date Received: 10/12/2018
Test Date: 10/15/2018
Valid Through: 10/15/2019

Sample #112339
Sample #112339 Sample #112339
Test
Compounds
CBDV* CBDA CBD CBC* CBG* CBN THC THCA THCV* Calc. Max THC Calc. Max CBD
Amount N/D 1.1% N/D N/D N/D N/D 6.4% 71.9% N/D 69.5% 1.0%
LOQ 0.3% 0.3% 0.3% 0.3% 0.3% 0.3% 0.3% 0.3% 0.3%
Uncertainty ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD

LOQ = Limit of Quantitation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates compounds that are not currently included in Iron Laboratories' accredited scope.

*** Designates tests that use the method FE-45.

Calc. Max is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the CBDA or THCA value.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories

Residual Solvents Analysis by
Mass Spectrometer

Test Certificate #: 112339-001
Client Name, Sample Details

Mitten Maid
Lansing, MI 48910
Sample: Yumbolt Nug Run Live Resin Badder
Type: Undiluted
Method: SOP FE-44-OR3

Test Conditions

Scale: XS205-MI1
Temp: 21.9 °C
Baro Pressure: 979.2 hPa
Analyst: HRM
Technician: ACR

Sample ID#: 112339

Harvest Date: 10/15/2018
Date Received: 10/12/2018

Sample #112339
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 150 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories

Terpene Report by
Mass Spectrometer

Test Certificate #: 112339-001
Client Name, Sample Details

Mitten Maid
Lansing, MI 48910
Sample: Yumbolt Nug Run Live Resin Badder
Type: Undiluted
Method: SOP FE-44-OR3

Test Conditions

Scale: XS205-MI1
Temp: 19.4 °C
Baro Pressure: 1008 hPa
Analyst: HRM
Technician: ACR

Sample ID#: 112339

Harvest Date: 10/15/2018
Date Received: 10/12/2018

Sample #112339

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.260 %

β-Ocimene:

0.160 %

Camphene:

0.030 %

Eucalyptol (1,8-Cineol):

0.020 %

Sabinene:

N/D

γ-Terpinene:

N/D

Myrcene:

0.290 %

α-Terpinolene:

0.050 %

β-Pinene:

0.230 %

Linalool:

0.090 %

∆3-Carene:

N/D

Fenchone:

0.020 %

α-Terpinene:

0.020 %

Fenchol:

0.060 %

Ocimene:

N/D

Isopulegol:

N/D

Limonene:

0.240 %

Geraniol:

N/D

4-Cymene:

N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

1.100 %

α-Humulene:

0.670 %

Nerolidol 1:

0.080 %

Nerolidol 2:

0.030 %

Guaiol:

0.740 %

Caryophyllene Oxide:

0.060 %

α-Bisabolol:

0.070 %

Other Terpenes

Total: 4.220%
a-Phellandrene = 0.02 % a-Terpineol = 0.07 % Valencene = 0.12 %

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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