ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 112099-001
Client Name, Sample Details

Roxy Farms
Creswell, OR 97426
Sample: RN
Type: Industrial Hemp
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: ORP181004a
Scale: XS205-OR1
Temp: 21.2 °C
Baro Pressure: 1001 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 112099

Lot #: R & D only
Batch #: 112099
Harvest/Process Date: 10/04/2018
Package Weight (g):1.755
Date Received: 10/04/2018
Test Date: 10/04/2018
Sample #112099
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) N/D 0.07 0.03 2.03 N/D 0.01 0.01 N/D 0.01 2.16 0.06 1.81 1.90
Amount (mg/g) N/D 0.73 0.28 20.32 N/D 0.07 0.09 N/D 0.06 21.55 0.64 18.10 18.96
Amount per Serving (mg) N\D N\D N\D N\D N\D N\D N\D N\D N\D 0.00 Serving Size~ (g): 0.00
LOQ (mg/g) 0.03 0.03 0.03 0.03 0.03 0.03 0.03 0.03 0.03   %Decarb. THC CBD
±%RPD 4.13 6.47 2.72 3.75 3.41 3.26 4.47 3.17 3.29 0 1

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 112099-001
Client Name, Sample Details

Roxy Farms
Creswell, OR 97426
Sample: RN
Type: Industrial Hemp
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: ORP181004a
Scale: XS205-OR1
Temp: 21.2 °C
Baro Pressure: 1001 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 112099

Lot #: R & D only
Batch #: 112099
Harvest/Process Date: 10/04/2018
Package Weight (g):1.755
Date Received: 10/04/2018
Test Date: 10/04/2018
Sample #112099
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5.84 6.27 107.36 6.48 110.96 3.29
Cannabidiolic Acid (CBDA) N.D. 5.26 5.75 109.32 5.97 113.50 3.75
Cannabigerol (CBG) N.D. 5.8 6.03 103.97 6.23 107.41 3.26
Cannabidiol (CBD) N.D. 5.37 5.81 108.19 5.97 111.17 2.72
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.88 6.21 105.61 6.41 109.01 3.17
Cannabinol (CBN) N.D. 5.66 5.77 101.94 5.97 105.48 3.41
Δ9-Tetrahydrocannabinol (THC) N.D. 5.3 5.46 103.02 5.69 107.36 4.13
Cannabichromene (CBC) N.D. 5.83 5.9 101.20 6.17 105.83 4.47
Tetrahydrocannabinolic acid (THCA) N.D. 5.39 5.68 105.38 6.06 112.43 6.47

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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