Full Report - 110222

Pesticide Analysis by
Mass Spectrometer

Test Certificate #: 110222-001

Client Name, Sample Details
Hemp For Fitness & Natural Happiness® Glenview, IL 60026 Sample: Kratom Red KR310718 Type: Other Cannabinoid Product Method: FE-52 (EN 15662 & AOAC 2007.01)

Test Conditions
Prepsheet ID#: MIPS180820a Scale: XS205-MI2 Temp: 22.6 °C Baro PE: 984.3 hPa Analyst: JER Technician: JER

Sample ID#: 110222
Harvest/Process Date: 08/30/2018 Date Received: 08/30/2018 Test Date: 08/22/2018 Valid Through: 08/22/2019 Report Issued: 08/30/2018

Compound	MRL (µg/g)	LOD (µg/g)	Status (µg/g)	Compound	MRL (µg/g)	LOD (µg/g)	Status (µg/g)
Aldicarb	0.400	0.124	Pass/<LOD	Abamectin****	0.500	0.124	Pass/<LOD
Acephate	0.400	0.124	Pass/<LOD	Acequinocyl	2.000	0.249	Pass/<LOD
Acetamiprid	0.200	0.124	Pass/<LOD	Azoxystrobin	0.200	0.124	Pass/<LOD
Bifenazate	0.200	0.124	Pass/<LOD	Bifenthrin	0.200	0.124	Pass/<LOD
Boscalid	0.400	0.124	Pass/<LOD	Carbaryl	0.200	0.124	Pass/<LOD
Carbofuran	0.200	0.124	Pass/<LOD	Chlorantraniliprole	0.200	0.124	Pass/<LOD
Chlorfenapyr	1.000	0.497	Pass/<LOD	Chlorpyrifos	0.200	0.124	Pass/<LOD
Clofentezine	0.200	0.124	Pass/<LOD	Cyfluthrin**	1.000	0.497	Pass/<LOD
Cypermethrin***	1.000	0.497	Pass/<LOD	Daminozide	1.000	0.124	Pass/<LOD
DDVP (Dichlorvos)	1.000	0.249	Pass/<LOD	Diazinon	0.200	0.124	Pass/<LOD
Dimethoate	0.200	0.124	Pass/<LOD	Ethoprophos	0.200	0.124	Pass/<LOD
Etofenprox	0.400	0.124	Pass/<LOD	Etoxazole	0.200	0.124	Pass/<LOD
Fenoxycarb	0.200	0.124	Pass/<LOD	Fenpyroximate	0.400	0.124	Pass/<LOD
Fipronil	0.400	0.124	Pass/<LOD	Flonicamid	1.000	0.124	Pass/<LOD
Fludioxonil	0.400	0.124	Pass/<LOD	Hexythiazox	1.000	0.124	Pass/<LOD
Imazalil	0.200	0.124	Pass/<LOD	Imidacloprid	0.400	0.124	Pass/<LOD
Kresoxim Methyl	0.400	0.124	Pass/<LOD	Malathion	0.200	0.124	Pass/<LOD
Metalaxyl	0.200	0.124	Pass/<LOD	Methiocarb	0.200	0.124	Pass/<LOD
Methomyl	0.400	0.124	Pass/<LOD	Methyl Parathion	0.200	0.124	Pass/<LOD
MGK-264‡	0.200	0.124	Pass/<LOD	Myclobutanil	0.200	0.124	Pass/<LOD
Naled	0.500	0.124	Pass/<LOD	Oxamyl	1.000	0.124	Pass/<LOD
Paclobutrazol	0.400	0.124	Pass/<LOD	Permethrins†	0.200	0.124	Pass/<LOD
Phosmet	0.200	0.124	Pass/<LOD	Piperonyl Butoxide	2.000	0.124	Pass/<LOD
Prallethrin	0.200	0.124	Pass/<LOD	Propiconazole	0.400	0.124	Pass/<LOD
Propoxur	0.200	0.124	Pass/<LOD	Pyrethrins*	1.000	0.124	Pass/<LOD
Pyridaben	0.200	0.124	Pass/<LOD	Spinosad*****	0.200	0.124	Pass/<LOD
Spiromesifen	0.200	0.124	Pass/<LOD	Spirotetramat	0.200	0.124	Pass/<LOD
Spiroxamine‡	0.400	0.124	Pass/<LOD	Tebuconazole	0.400	0.124	Pass/<LOD
Thiacloprid	0.200	0.124	Pass/<LOD	Thiamethoxam	0.200	0.124	Pass/<LOD
Trifloxystrobin	0.200	0.124	Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Page 1 of 2

Pesticide QC Report

Test Certificate #: 110222-001

Client Name, Sample Details
Hemp For Fitness & Natural Happiness® Glenview, IL 60026 Sample: Kratom Red KR310718 Type: Other Cannabinoid Product Method: FE-52 (EN 15662 & AOAC 2007.01)

Test Conditions
Prepsheet ID#: MIPS180820a Scale: XS205-MI2 Temp: 22.6 °C Baro PE: 984.3 hPa Analyst: JER Technician: JER

Sample ID#: 110222
Harvest/Process Date: 08/30/2018 Date Received: 08/30/2018 Test Date: 08/22/2018 Valid Through: 08/22/2019 Report Issued: 08/30/2018

Target Compound Name	Method Blank (μg/g)	QC Spike (μg/g)	Matrix Spike (μg/g)	Matrix Spike Duplicate (μg/g)	MS recovery%	MSD recovery%	Relative Percent Difference (%)	QC Flag
Acephate	N.D.	1	0.892	1.07	89.20	107.00	18.14
Acequinocyl	N.D.	1	0.693	0.858	69.30	85.80	21.28	LRQ
Acetamiprid	N.D.	1	1	1.22	100.00	122.00	19.82
Aldicarb	N.D.	1	0.978	1.08	97.80	108.00	9.91
Avermectin B1a	N.D.	0.97	0.983	1.19	101.34	122.68	19.05
Azoxystrobin	N.D.	1	1.01	1.04	101.00	104.00	2.93
Bifenazate	N.D.	1	0.841	1.02	84.10	102.00	19.24
Bifenthrin	N.D.	1	1.11	1.11	111.00	111.00	0.00
Boscalid	N.D.	1	0.966	1.06	96.60	106.00	9.28
Carbaryl	N.D.	1	0.991	1.28	99.10	128.00	25.45	Q
Carbofuran	N.D.	1	1.02	1.11	102.00	111.00	8.45
Chlorantraniliprole	N.D.	1	1.06	1.16	106.00	116.00	9.01
Chlorfenapyr	N.D.	1	1.14	1.16	114.00	116.00	1.74
Chlorpyriphos	N.D.	1	1.02	1.16	102.00	116.00	12.84
Clofentezine	N.D.	1	0.953	0.888	95.30	88.80	7.06
Cyfluthrin	N.D.	1	1.05	1.05	105.00	105.00	0.00
Cypermethrin	N.D.	1	0.829	1.27	82.90	127.00	42.02	Q
Daminoside	N.D.	1	0.759	0.86	75.90	86.00	12.48
Diazanon	N.D.	1	1.25	1.37	125.00	137.00	9.16	HR
Dichlorvos	N.D.	1	1.04	1.19	104.00	119.00	13.45
Dimethoate	N.D.	1	0.981	1.08	98.10	108.00	9.61
Ethoprophos	N.D.	1	0.971	1.01	97.10	101.00	3.94
Etofenprox	N.D.	0	0	0	nan	nan
Etoxazole	N.D.	1	1.15	1.19	115.00	119.00	3.42
Fenoxycarb	N.D.	1	1.08	1.12	108.00	112.00	3.64
Fenpyroximate	N.D.	1	1.12	1.15	112.00	115.00	2.64
Fipronil	N.D.	1	1.24	1.07	124.00	107.00	14.72
Flonicamid	N.D.	1	0.94	1.18	94.00	118.00	22.64	Q
Fludioxonil	N.D.	1	1.12	0.906	112.00	90.60	21.13	Q
Hexythiazox	N.D.	1	0.982	1.08	98.20	108.00	9.51
Imazalil	N.D.	1	1.02	1.09	102.00	109.00	6.64
Imidacloprid	N.D.	1	0.966	1.04	96.60	104.00	7.38
Kresoxim-methyl	N.D.	1	0.917	1.21	91.70	121.00	27.55	Q
Malathion	N.D.	1	1.14	1.07	114.00	107.00	6.33
Metalaxyl	N.D.	1	1.03	1.07	103.00	107.00	3.81
Methiocarb	N.D.	1	1.05	1.18	105.00	118.00	11.66
Methomyl	N.D.	1	1.05	1.29	105.00	129.00	20.51	Q
MGK-264	N.D.	1	1.01	1.03	101.00	103.00	1.96
Myclobutanil	N.D.	1	0.988	0.967	98.80	96.70	2.15
Naled (dibrom)	N.D.	1	0.818	0.888	81.80	88.80	8.21
Oxamyl	N.D.	1	1.08	1.15	108.00	115.00	6.28
Paclobutrazol	N.D.	1	1.03	1.16	103.00	116.00	11.87
Parathion-methyl	N.D.	1	1.2	0.935	120.00	93.50	24.82	Q
Permethrins	N.D.	1	1.15	1.21	115.00	121.00	5.08
Phosmet	N.D.	1	1.04	1.06	104.00	106.00	1.90
Piperonyl butoxide	N.D.	1	1.03	1.08	103.00	108.00	4.74
Prallethrin	N.D.	1	1.15	1.09	115.00	109.00	5.36
Propiconazole	N.D.	1	0.91	1.05	91.00	105.00	14.29
Propoxur	N.D.	1	0.917	1.1	91.70	110.00	18.15
Pyrethrin	N.D.	0.65	0.619	0.661	95.23	101.69	6.56
Pyridaben	N.D.	0	0	0	nan	nan
SpinosynA	N.D.	0.84	0.713	0.817	84.88	97.26	13.59
SpinosynD	N.D.	0	0	0	nan	nan
Spiromesifen	N.D.	1	0.372	0.458	37.20	45.80	20.72	LRQ
Spirotetramat	N.D.	1	0.937	0.953	93.70	95.30	1.69
Spiroxamine	N.D.	1	0.973	1.13	97.30	113.00	14.93
Tebuconazole	N.D.	1	1.06	1.16	106.00	116.00	9.01
Thiacloprid	N.D.	1	0.989	1.12	98.90	112.00	12.42
Thiamethoxam	N.D.	1	0.911	1.24	91.10	124.00	30.59	Q
Trifloxystrobin	N.D.	1	0.996	1.17	99.60	117.00	16.07

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Page 2 of 2

Pesticide Analysis byMass Spectrometer

Client Name, Sample Details

Test Conditions

Sample ID#: 110222

Pesticide QC Report

Client Name, Sample Details

Test Conditions

Sample ID#: 110222

Pesticide Analysis by
Mass Spectrometer