IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 136722-001
Client Name, Sample Details

Synergy Leaf Tea
Northville, MI 48167
Sample: Sleep and Serenitea
Type: Infused Product
Method: FE04U12 HPLC-UV

Test Conditions

Prepsheet ID#: MIP220503A
Scale: XS205-MI2
Temp: 21.3 °C
Baro Pressure: 984.3 hPa
Analyst: SKM
Technician: SKM

Sample ID#: 136722

Harvest/Process Date: 05/04/2022
Serving Size (g): 3.92
Date Received: 05/04/2022
Test Date: 05/03/2022
Valid Through: 05/04/2023
Report Issued: 05/04/2022

Sample #136722
Sample #136722 Sample #136722
Test
Compounds
Δ9-THC THCA Δ8-THC CBD CBDA CBG CBGA CBN CBC CBL THCV CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) N/D N/D N/D 0.5 N/D N/D N/D N/D N/D N/D N/D N/D 0.5 N/D 0.5 0.5
Amount (mg/g) N/D N/D N/D 5.2 N/D 0.2 N/D N/D N/D N/D N/D N/D 5.4 N/D 5.2 5.4
Amount per Serving (mg) N/D N/D N/D 20.384 N/D 0.784 N/D N/D N/D N/D N/D N/D 21.2 Serving Size~ (g): 3.9
LOQ (mg/g) 0.03 0.03 0.03 0.03 0.03 0.03 0.03 0.03 0.03 0.03 0.03 0.03   %Decarb. THC CBD
±%RPD 0.08% 0.27% 2.18% 2.61% 0.12% 0.86% 0.98% 1.89% 0.70% 2.56% 1.70% 0.10% N/A 100%

Serving size = 1 teabag = 3.92g.

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009.

FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products.

Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of Δ9-THC and Δ8-THC or CBD plus the amount of THC or CBD derived from THCA or CBDA, respectively.

These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value.

Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, Total CBG, CBC, THCV, CBDV, and CBL.

Total CBG is calculated as CBG plus CBGA*0.878 (the molar correction factor for CBGA to CBG conversion).

%Decarb. THC and CBD refer to the percentage of Δ9-THC or CBD relative to THCA or CBDA, respectively.

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 136722-001
Client Name, Sample Details

Synergy Leaf Tea
Northville, MI 48167
Sample: Sleep and Serenitea
Type: Infused Product
Method: FE04U12 HPLC-UV

Test Conditions

Prepsheet ID#: MIP220503A
Scale: XS205-MI2
Temp: 21.3 °C
Baro Pressure: 984.3 hPa
Analyst: SKM
Technician: SKM

Sample ID#: 136722

Harvest/Process Date: 05/04/2022
Serving Size (g): 3.92
Date Received: 05/04/2022
Test Date: 05/03/2022
Valid Through: 05/04/2023
Report Issued: 05/04/2022

Sample #136722
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Δ9-THC 0 5.38933832 5.705654128 105.87 5.71015547 105.95 0.08%
THCA 0 4.802686133 5.128835711 106.79 5.114765801 106.50 0.27%
Δ8-THC 0 5.367189658 5.625914063 104.82 5.749768489 107.13 2.18%
CBD 0 5.611169191 5.887892483 104.93 5.736438988 102.23 2.61%
CBDA 0 4.807384026 5.109367369 106.28 5.10303283 106.15 0.12%
CBG 0 5.93543644 6.279325976 105.79 6.225538073 104.89 0.86%
CBGA 0 5.017490265 5.317249707 105.97 5.265331972 104.94 0.98%
CBN 0 5.138660732 5.579278821 108.57 5.474886968 106.54 1.89%
CBC 0 5.579993981 5.864807121 105.10 5.823647186 104.37 0.70%
CBCA N/A N/A N/A nan N/A nan 0%
CBL 0 5.475323993 5.851606731 106.87 5.7035506 104.17 2.56%
THCV 0 5.538285688 5.907708961 106.67 5.808066113 104.87 1.70%
CBDV 0 5.488473652 5.818355752 106.01 5.824355659 106.12 0.10%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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